octane-1,4,7-triyl triacetate

Base Information

• Chemical Name: octane-1,4,7-triyl triacetate
• CAS No.: 5451-24-1
• Molecular Formula: C14H24 O6
• Molecular Weight: 288.341
• Mol file: 5451-24-1.mol

Synonyms:1,4,7-Octanetriol,triacetate (7CI,8CI); NSC 18539

Chemical Property of octane-1,4,7-triyl triacetate

Chemical Property:

• Vapor Pressure: 2.91E-05mmHg at 25°C
• Boiling Point: 356.5°Cat760mmHg
• Flash Point: 152.7°C
• Density: 1.064g/cm³

Purity/Quality:

99%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of octane-1,4,7-triyl triacetate

There total 4 articles about octane-1,4,7-triyl triacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-(furan-2-yl)but-3-en-2-one (623-15-4) + acetic acid (64-19-7,77671-22-8) → octane (111-65-9) + n-octyl acetate (112-14-1) + octane-1,4,7-triyl triacetate (5451-24-1)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; zinc trifluoromethanesulfonate; at 150 ℃; for 2h; under 15001.5 Torr; Reagent/catalyst; Autoclave; Green chemistry;

DOI:10.1039/c9gc01767d

Reference yield:

4-(furan-2-yl)but-3-en-2-one (623-15-4) + acetic acid (64-19-7,77671-22-8) → 4-(tetrahydrofuran-2-yl)butan-2-yl acetate (91006-98-3) + octane (111-65-9) + n-octyl acetate (112-14-1) + octane-1,4,7-triyl triacetate (5451-24-1)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; lanthanum(lll) triflate; at 150 ℃; for 2h; under 15001.5 Torr; Autoclave; Green chemistry;

DOI:10.1039/c9gc01767d

Reference yield:

4-(furan-2-yl)but-3-en-2-one (623-15-4) + acetic acid (64-19-7,77671-22-8) → n-octyl acetate (112-14-1) + octane-1,4,7-triyl triacetate (5451-24-1)

Guidance literature:

With bismuth(lll) trifluoromethanesulfonate; palladium 10% on activated carbon; hydrogen; at 150 ℃; for 2h; under 15001.5 Torr; Autoclave; Green chemistry;

DOI:10.1039/c9gc01767d

upstream raw materials:

4-(furan-2-yl)but-3-en-2-one

acetic acid

Downstream raw materials:

n-octyl acetate

Refernces