4-(tetrahydrofuran-2-yl)butan-2-yl acetate

Base Information

• Chemical Name: 4-(tetrahydrofuran-2-yl)butan-2-yl acetate
• CAS No.: 91006-98-3
• Molecular Formula: C₁₀H₁₈O₃
• Molecular Weight: 186.251
• Mol file: 91006-98-3.mol

Synonyms:4-(tetrahydrofuran-2-yl)butan-2-yl acetate

Chemical Property of 4-(tetrahydrofuran-2-yl)butan-2-yl acetate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 4-(tetrahydrofuran-2-yl)butan-2-yl acetate

There total 2 articles about 4-(tetrahydrofuran-2-yl)butan-2-yl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-(furan-2-yl)but-3-en-2-one (623-15-4) + acetic acid (64-19-7,77671-22-8) → 4-(tetrahydrofuran-2-yl)butan-2-yl acetate (91006-98-3) + octane (111-65-9) + n-octyl acetate (112-14-1) + octane-1,4,7-triyl triacetate (5451-24-1)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; lanthanum(lll) triflate; at 150 ℃; for 2h; under 15001.5 Torr; Autoclave; Green chemistry;

DOI:10.1039/c9gc01767d

Reference yield:

4-(furan-2-yl)but-3-en-2-one (623-15-4) + acetic acid (64-19-7,77671-22-8) → 4-(tetrahydrofuran-2-yl)butan-2-yl acetate (91006-98-3) + n-octyl acetate (112-14-1) + octane-1,4,7-triyl triacetate (5451-24-1)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; scandium tris(trifluoromethanesulfonate); at 150 ℃; for 2h; under 15001.5 Torr; Autoclave; Green chemistry;

DOI:10.1039/c9gc01767d

Reference yield:

4-(tetrahydrofuran-2-yl)butan-2-yl acetate (91006-98-3) → n-octyl acetate (112-14-1)

Guidance literature:

Multi-step reaction with 2 steps

1: scandium tris(trifluoromethanesulfonate) / 150 °C

2: palladium 10% on activated carbon; hydrogen; scandium tris(trifluoromethanesulfonate) / 150 °C / 15001.5 Torr / Autoclave

With palladium 10% on activated carbon; hydrogen; scandium tris(trifluoromethanesulfonate);

DOI:10.1039/c9gc01767d

upstream raw materials:

4-(furan-2-yl)but-3-en-2-one

acetic acid

Downstream raw materials:

n-octyl acetate