(S)-(-)-menthyl [(R)-1-(4-bromophenyl)-1-hydroxyethyl]phenylphosphinate

Base Information

Chemical Name:(S)-(-)-menthyl [(R)-1-(4-bromophenyl)-1-hydroxyethyl]phenylphosphinate
CAS No.:1610879-65-6
Molecular Formula:C₂₄H₃₂BrO₃P
Molecular Weight:479.394
Hs Code.:

Synonyms:(S)-(-)-menthyl [(R)-1-(4-bromophenyl)-1-hydroxyethyl]phenylphosphinate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-(-)-menthyl [(R)-1-(4-bromophenyl)-1-hydroxyethyl]phenylphosphinate

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Technology Process of (S)-(-)-menthyl [(R)-1-(4-bromophenyl)-1-hydroxyethyl]phenylphosphinate

There total 4 articles about (S)-(-)-menthyl [(R)-1-(4-bromophenyl)-1-hydroxyethyl]phenylphosphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 99-90-1
para-bromoacetophenone

: 31352-60-0,31352-61-1,54353-18-3
(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl phenylphosphinate

: 1610879-65-6
(S)-(-)-menthyl [(R)-1-(4-bromophenyl)-1-hydroxyethyl]phenylphosphinate

Guidance literature:: With potassium carbonate; In dimethyl sulfoxide; at 20 ℃; for 24h; Time; diastereoselective reaction;
DOI:10.1002/asia.201301650

Reference yield:

: 99-90-1
para-bromoacetophenone

: 31352-60-0,31352-61-1,54353-18-3
(1R,2S,5R)-5-methyl-2-(propan-2-yl)cyclohexyl phenylphosphinate

: 1610879-65-6
(S)-(-)-menthyl [(R)-1-(4-bromophenyl)-1-hydroxyethyl]phenylphosphinate

Guidance literature:: With potassium carbonate; In dimethyl sulfoxide; at 20 ℃; for 24h; Solvent; Temperature; Reagent/catalyst; Time;
DOI:10.1039/c4ob01574f

Reference yield:

: 99-90-1
para-bromoacetophenone

: 31352-60-0,31352-61-1,54353-18-3
(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl phenylphosphinate

: 1610879-65-6
(S)-(-)-menthyl [(R)-1-(4-bromophenyl)-1-hydroxyethyl]phenylphosphinate

: 1610880-25-5
(S)-(-)-menthyl [(S)-1-(4-bromophenyl)-1-hydroxyethyl]phenylphosphinate

Guidance literature:: With potassium carbonate; In dimethyl sulfoxide; at 20 ℃; for 10h; Time; Overall yield = 97 %; diastereoselective reaction;
DOI:10.1002/asia.201301650