(S_P)-(1R,2S,5R)-2-Isopropyl-5-methylcyclohexyl phenylphosphinate

Base Information

Chemical Name:(S_P)-(1R,2S,5R)-2-Isopropyl-5-methylcyclohexyl phenylphosphinate
CAS No.:31352-60-0
Molecular Formula:C₁₆H₂₅O₂P
Molecular Weight:280.347
Hs Code.:

(S<SUB>P</SUB>)-(1R,2S,5R)-2-Isopropyl-5-methylcyclohexyl phenylphosphinate

Synonyms:

Suppliers and Price of (S_P)-(1R,2S,5R)-2-Isopropyl-5-methylcyclohexyl phenylphosphinate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemicals and raw materials
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Total 2 raw suppliers

Chemical Property of (S_P)-(1R,2S,5R)-2-Isopropyl-5-methylcyclohexyl phenylphosphinate

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of (S_P)-(1R,2S,5R)-2-Isopropyl-5-methylcyclohexyl phenylphosphinate

There total 29 articles about (S_P)-(1R,2S,5R)-2-Isopropyl-5-methylcyclohexyl phenylphosphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.6%

: 824-72-6
P,P-dichlorophenylphosphine oxide

: 2216-51-5
(-)-menthol

: 31352-60-0,31352-61-1,54353-18-3
(1R,2S,5R)-5-methyl-2-(propan-2-yl)cyclohexyl phenylphosphinate

: (-)-menthyl chloride

Guidance literature:: In dichloromethane; at 20 ℃; for 12h;
DOI:10.1002/hc.10150

Reference yield: 99.0%

: 14602-86-9,7635-53-2
(1R,2S,5R)-menthyl chloroformate

: 1779-48-2
phenylphosphinic acid

: 31352-60-0,31352-61-1,54353-18-3
(1R,2S,5R)-5-methyl-2-(propan-2-yl)cyclohexyl phenylphosphinate

Guidance literature:: With pyridine; In toluene; Heating;
DOI:10.1016/S0040-4039(02)02647-3

Reference yield: 91.0%

: 1508260-88-5
(S_p)-menthyl (hydroxymethyl)phenylphosphinate

: 31352-60-0,31352-61-1,54353-18-3
(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl phenylphosphinate

Guidance literature:: (S_p)-menthyl (hydroxymethyl)phenylphosphinate; With N-chloro-succinimide; dimethylsulfide; In dichloromethane; at -78 ℃; for 1.33333h; Inert atmosphere;

With triethylamine; In dichloromethane; at -78 - 20 ℃; for 1.25h; stereoselective reaction; Inert atmosphere;
DOI:10.1002/anie.201306628