anti-β-N-(S)-(-)-2-methoxymethylpyrrolidineimino propyldiphenylphosphine oxide

Base Information

Chemical Name:anti-β-N-(S)-(-)-2-methoxymethylpyrrolidineimino propyldiphenylphosphine oxide
CAS No.:150712-46-2
Molecular Formula:C₂₁H₂₇N₂O₂P
Molecular Weight:370.431
Hs Code.:

Synonyms:anti-β-N-(S)-(-)-2-methoxymethylpyrrolidineimino propyldiphenylphosphine oxide

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Chemical Property of anti-β-N-(S)-(-)-2-methoxymethylpyrrolidineimino propyldiphenylphosphine oxide

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Technology Process of anti-β-N-(S)-(-)-2-methoxymethylpyrrolidineimino propyldiphenylphosphine oxide

There total 1 articles about anti-β-N-(S)-(-)-2-methoxymethylpyrrolidineimino propyldiphenylphosphine oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13172-76-4
diphenyl(propa-1,2-dien-1-yl)phosphine oxide

: 59983-39-0,187035-29-6
(S)-1-amino-2-(methoxymethyl)pyrrolidine

: 167252-45-1
syn-β-N-(S)-(-)-2-methoxymethylpyrrolidineimino propyldiphenylphosphine oxide

: 150712-46-2
anti-β-N-(S)-(-)-2-methoxymethylpyrrolidineimino propyldiphenylphosphine oxide

Guidance literature:: In chloroform; Yields of byproduct given. Title compound not separated from byproducts; Heating;
DOI:10.1016/S0040-4020(01)89404-7

Reference yield: 84.0%

: 106-96-7
propargyl bromide

: 150712-46-2
anti-β-N-(S)-(-)-2-methoxymethylpyrrolidineimino propyldiphenylphosphine oxide

: [2-(Diphenyl-phosphinoyl)-1-methyl-pent-4-yn-(E)-ylidene]-((S)-2-methoxymethyl-pyrrolidin-1-yl)-amine

Guidance literature:: anti-β-N-(S)-(-)-2-methoxymethylpyrrolidineimino propyldiphenylphosphine oxide; With lithium diisopropyl amide; In tetrahydrofuran; hexane; at -78 ℃; for 1h;

propargyl bromide; In tetrahydrofuran; hexane; at -78 - 20 ℃;
DOI:10.1016/S0040-4020(01)00033-3

Reference yield: 67.0%

: 105-36-2
ethyl bromoacetate

: 150712-46-2
anti-β-N-(S)-(-)-2-methoxymethylpyrrolidineimino propyldiphenylphosphine oxide

: 3-(Diphenyl-phosphinoyl)-4-[(E)-(S)-2-methoxymethyl-pyrrolidin-1-ylimino]-pentanoic acid ethyl ester

Guidance literature:: anti-β-N-(S)-(-)-2-methoxymethylpyrrolidineimino propyldiphenylphosphine oxide; With copper(l) iodide; n-butyllithium; In tetrahydrofuran; diethyl ether; hexane; at -50 ℃; for 1h;

ethyl bromoacetate; In tetrahydrofuran; diethyl ether; hexane; at -50 - -30 ℃;
DOI:10.1016/S0040-4020(01)00033-3