(3R,4S,5S,6R)-2,7-bis[[4-(methoxycarbonyl)phenyl]methyl]-4,5-bis[(2-methoxyethoxy)methoxy]-3,6-bis(phenoxymethyl)-1,2,7-thiadiazepine 1,1-dioxide

Base Information

• Chemical Name: (3R,4S,5S,6R)-2,7-bis[[4-(methoxycarbonyl)phenyl]methyl]-4,5-bis[(2-methoxyethoxy)methoxy]-3,6-bis(phenoxymethyl)-1,2,7-thiadiazepine 1,1-dioxide
• CAS No.: 247233-85-8
• Molecular Formula: C₄₄H₅₄N₂O₁₄S
• Molecular Weight: 866.984

Synonyms:(3R,4S,5S,6R)-2,7-bis[[4-(methoxycarbonyl)phenyl]methyl]-4,5-bis[(2-methoxyethoxy)methoxy]-3,6-bis(phenoxymethyl)-1,2,7-thiadiazepine 1,1-dioxide

Chemical Property of (3R,4S,5S,6R)-2,7-bis[[4-(methoxycarbonyl)phenyl]methyl]-4,5-bis[(2-methoxyethoxy)methoxy]-3,6-bis(phenoxymethyl)-1,2,7-thiadiazepine 1,1-dioxide

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Technology Process of (3R,4S,5S,6R)-2,7-bis[[4-(methoxycarbonyl)phenyl]methyl]-4,5-bis[(2-methoxyethoxy)methoxy]-3,6-bis(phenoxymethyl)-1,2,7-thiadiazepine 1,1-dioxide

There total 1 articles about (3R,4S,5S,6R)-2,7-bis[[4-(methoxycarbonyl)phenyl]methyl]-4,5-bis[(2-methoxyethoxy)methoxy]-3,6-bis(phenoxymethyl)-1,2,7-thiadiazepine 1,1-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

Methyl 4-(bromomethyl)benzoate (2417-72-3) + (3R,4S,5S,6R)-4,5-Bis-(2-methoxy-ethoxymethoxy)-3,6-bis-phenoxymethyl-[1,2,7]thiadiazepane 1,1-dioxide (185450-20-8) → (3R,4S,5S,6R)-2,7-bis[[4-(methoxycarbonyl)phenyl]methyl]-4,5-bis[(2-methoxyethoxy)methoxy]-3,6-bis(phenoxymethyl)-1,2,7-thiadiazepine 1,1-dioxide (247233-85-8)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide;

DOI:10.1021/jm991054q

Reference yield: 80.0%

(3R,4S,5S,6R)-2,7-bis[[4-(methoxycarbonyl)phenyl]methyl]-4,5-bis[(2-methoxyethoxy)methoxy]-3,6-bis(phenoxymethyl)-1,2,7-thiadiazepine 1,1-dioxide (247233-85-8) → C36H38N2O10S

Guidance literature:

With hydrogenchloride; In diethyl ether;

DOI:10.1021/jm991054q

Reference yield:

(3R,4S,5S,6R)-2,7-bis[[4-(methoxycarbonyl)phenyl]methyl]-4,5-bis[(2-methoxyethoxy)methoxy]-3,6-bis(phenoxymethyl)-1,2,7-thiadiazepine 1,1-dioxide (247233-85-8) → {4-[(3R,4S,5S,6R)-7-(4-Hydroxymethyl-benzyl)-4,5-bis-(2-methoxy-ethoxymethoxy)-1,1-dioxo-3,6-bis-phenoxymethyl-1λ6-[1,2,7]thiadiazepan-2-ylmethyl]-phenyl}-methanol

Guidance literature:

With lithium borohydride; In diethyl ether; toluene; at 80 ℃; for 2h;

DOI:10.1021/jm991054q

upstream raw materials:

Methyl 4-(bromomethyl)benzoate

(3R,4S,5S,6R)-4,5-Bis-(2-methoxy-ethoxymethoxy)-3,6-bis-phenoxymethyl-[1,2,7]thiadiazepane 1,1-dioxide

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