C₂₉H₂₈FN₃O₅

Base Information

Chemical Name:C₂₉H₂₈FN₃O₅
CAS No.:1204423-84-6
Molecular Formula:C₂₉H₂₈FN₃O₅
Molecular Weight:517.557
Hs Code.:

C<sub>29</sub>H<sub>28</sub>FN<sub>3</sub>O<sub>5</sub>

Synonyms:C₂₉H₂₈FN₃O₅

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Chemical Property of C₂₉H₂₈FN₃O₅

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Technology Process of C₂₉H₂₈FN₃O₅

There total 11 articles about C₂₉H₂₈FN₃O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1204423-83-5
C₂₇H₂₅BrFN₃O₅

: 7486-35-3
tri-n-butyl(vinyl)tin

: 1204423-84-6
C₂₉H₂₈FN₃O₅

Guidance literature:: C₂₇H₂₅BrFN₃O₅; tri-n-butyl(vinyl)tin; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; at 110 ℃; for 3h;

With potassium fluoride dihydrate; In water; toluene; at 20 ℃; for 1h;

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 1204423-84-6
C₂₉H₂₈FN₃O₅

Guidance literature:: Multi-step reaction with 9 steps

1.1: hydroxylamine hydrochloride; sodium hydrogencarbonate / ethanol / 1 h / 20 °C

2.1: N-chloro-succinimide / N,N-dimethyl-formamide / 2.5 h / 20 °C / Cooling with ice

3.1: triethylamine / dichloromethane / 2 h / 20 °C

4.1: carbon tetrabromide; triphenylphosphine / dichloromethane / 1 h / Cooling with ice

5.1: potassium tert-butylate / N,N-dimethyl-formamide / 0.17 h / 20 °C

5.2: 1 h / 20 °C

6.1: N-Bromosuccinimide / N,N-dimethyl-formamide / 13 h / 20 °C

7.1: sodium hydroxide; water / ethanol / 1 h / 20 °C

7.3: 8 h / 130 °C

8.1: triethylamine; HATU / N,N-dimethyl-formamide / 1 h / 0 - 20 °C

9.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 3 h / 110 °C

9.2: 1 h / 20 °C

With N-chloro-succinimide; N-Bromosuccinimide; carbon tetrabromide; hydroxylamine hydrochloride; potassium tert-butylate; water; sodium hydrogencarbonate; triethylamine; triphenylphosphine; HATU; sodium hydroxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; dichloromethane; N,N-dimethyl-formamide; toluene;

Reference yield:

: 3717-21-3,3717-22-4,140461-28-5,140461-29-6,3235-04-9
p-methoxyl benzaldoxime

: 1204423-84-6
C₂₉H₂₈FN₃O₅

Guidance literature:: Multi-step reaction with 8 steps

1.1: N-chloro-succinimide / N,N-dimethyl-formamide / 2.5 h / 20 °C / Cooling with ice

2.1: triethylamine / dichloromethane / 2 h / 20 °C

3.1: carbon tetrabromide; triphenylphosphine / dichloromethane / 1 h / Cooling with ice

4.1: potassium tert-butylate / N,N-dimethyl-formamide / 0.17 h / 20 °C

4.2: 1 h / 20 °C

5.1: N-Bromosuccinimide / N,N-dimethyl-formamide / 13 h / 20 °C

6.1: sodium hydroxide; water / ethanol / 1 h / 20 °C

6.3: 8 h / 130 °C

7.1: triethylamine; HATU / N,N-dimethyl-formamide / 1 h / 0 - 20 °C

8.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 3 h / 110 °C

8.2: 1 h / 20 °C

With N-chloro-succinimide; N-Bromosuccinimide; carbon tetrabromide; potassium tert-butylate; water; triethylamine; triphenylphosphine; HATU; sodium hydroxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; dichloromethane; N,N-dimethyl-formamide; toluene;