(S)-2-[(S)-2-((S)-2-Amino-4-methylsulfanyl-butyrylamino)-4-methyl-pentanoylamino]-3-phenyl-propionic acid (benzhydryl-carbamoyl)-methyl ester; compound with trifluoro-acetic acid

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Chemical Name:(S)-2-[(S)-2-((S)-2-Amino-4-methylsulfanyl-butyrylamino)-4-methyl-pentanoylamino]-3-phenyl-propionic acid (benzhydryl-carbamoyl)-methyl ester; compound with trifluoro-acetic acid
CAS No.:119724-66-2
Molecular Formula:C₂HF₃O₂*C₃₅H₄₄N₄O₅S
Molecular Weight:746.848
Hs Code.:

(S)-2-[(S)-2-((S)-2-Amino-4-methylsulfanyl-butyrylamino)-4-methyl-pentanoylamino]-3-phenyl-propionic acid (benzhydryl-carbamoyl)-methyl ester; compound with trifluoro-acetic acid

Synonyms:(S)-2-[(S)-2-((S)-2-Amino-4-methylsulfanyl-butyrylamino)-4-methyl-pentanoylamino]-3-phenyl-propionic acid (benzhydryl-carbamoyl)-methyl ester; compound with trifluoro-acetic acid

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Chemical Property of (S)-2-[(S)-2-((S)-2-Amino-4-methylsulfanyl-butyrylamino)-4-methyl-pentanoylamino]-3-phenyl-propionic acid (benzhydryl-carbamoyl)-methyl ester; compound with trifluoro-acetic acid

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Technology Process of (S)-2-[(S)-2-((S)-2-Amino-4-methylsulfanyl-butyrylamino)-4-methyl-pentanoylamino]-3-phenyl-propionic acid (benzhydryl-carbamoyl)-methyl ester; compound with trifluoro-acetic acid

There total 1 articles about (S)-2-[(S)-2-((S)-2-Amino-4-methylsulfanyl-butyrylamino)-4-methyl-pentanoylamino]-3-phenyl-propionic acid (benzhydryl-carbamoyl)-methyl ester; compound with trifluoro-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 119724-63-9
Boc-Met-Leu-Phe-OBg

: 76-05-1
trifluoroacetic acid

: 119724-66-2
(S)-2-[(S)-2-((S)-2-Amino-4-methylsulfanyl-butyrylamino)-4-methyl-pentanoylamino]-3-phenyl-propionic acid (benzhydryl-carbamoyl)-methyl ester; compound with trifluoro-acetic acid

Guidance literature:: for 0.5h; Yield given; Ambient temperature;
DOI:10.1016/S0040-4020(01)86014-2

Reference yield: 92.0%

: 33104-36-8
2,4,5-trichlorophenylformiate

: 119724-66-2
(S)-2-[(S)-2-((S)-2-Amino-4-methylsulfanyl-butyrylamino)-4-methyl-pentanoylamino]-3-phenyl-propionic acid (benzhydryl-carbamoyl)-methyl ester; compound with trifluoro-acetic acid

: 119706-26-2
For-Met-Leu-Phe-OBg

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; for 0.25h; Ambient temperature;
DOI:10.1016/S0040-4020(01)86014-2

Reference yield:

: 119724-66-2
(S)-2-[(S)-2-((S)-2-Amino-4-methylsulfanyl-butyrylamino)-4-methyl-pentanoylamino]-3-phenyl-propionic acid (benzhydryl-carbamoyl)-methyl ester; compound with trifluoro-acetic acid

: 59880-97-6
formyl-methionyl-leucyl-phenylalanine

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / DIEA / dimethylformamide / 0.25 h / Ambient temperature

2: 91 percent / potassium carbonate / H₂O; dimethylformamide / 0.5 h / Ambient temperature

With potassium carbonate; N-ethyl-N,N-diisopropylamine; In water; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)86014-2