4-bromo-2-(α-ethoxy-4-chlorobenzyl)-5-(trifluoromethyl)-1H-pyrrole-3-carbonitrile

Base Information

Chemical Name:4-bromo-2-(α-ethoxy-4-chlorobenzyl)-5-(trifluoromethyl)-1H-pyrrole-3-carbonitrile
CAS No.:1614231-68-3
Molecular Formula:C₁₅H₁₁BrClF₃N₂O
Molecular Weight:407.617
Hs Code.:

Synonyms:4-bromo-2-(α-ethoxy-4-chlorobenzyl)-5-(trifluoromethyl)-1H-pyrrole-3-carbonitrile

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Chemical Property of 4-bromo-2-(α-ethoxy-4-chlorobenzyl)-5-(trifluoromethyl)-1H-pyrrole-3-carbonitrile

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Technology Process of 4-bromo-2-(α-ethoxy-4-chlorobenzyl)-5-(trifluoromethyl)-1H-pyrrole-3-carbonitrile

There total 4 articles about 4-bromo-2-(α-ethoxy-4-chlorobenzyl)-5-(trifluoromethyl)-1H-pyrrole-3-carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 64-17-5
ethanol

: 1614231-65-0
4-bromo-2-(α-chloro-4-chlorobenzyl)-5-(trifluoromethyl)-1H-pyrrole-3-carbonitrile

: 1614231-68-3
4-bromo-2-(α-ethoxy-4-chlorobenzyl)-5-(trifluoromethyl)-1H-pyrrole-3-carbonitrile

Guidance literature:: With sodium carbonate; for 1h; Reflux;
DOI:10.1021/jf501377t

Reference yield:

: 1614231-61-6
C₁₃H₇BrClF₃N₂

: 1614231-68-3
4-bromo-2-(α-ethoxy-4-chlorobenzyl)-5-(trifluoromethyl)-1H-pyrrole-3-carbonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 12 h / 20 °C / Reflux

2: sodium carbonate / 1 h / Reflux

With sodium carbonate; In dichloromethane;
DOI:10.1021/jf501377t

Reference yield:

: 1614231-63-8
4-bromo-2-(α-hydroxyl-4-chlorobenzyl)-5-(trifluoromethyl)-1H-pyrrole-3-carbonitrile

: 1614231-68-3
4-bromo-2-(α-ethoxy-4-chlorobenzyl)-5-(trifluoromethyl)-1H-pyrrole-3-carbonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuryl dichloride / dichloromethane / 8 h / Reflux

2: sodium carbonate / 1 h / Reflux

With sulfuryl dichloride; sodium carbonate; In dichloromethane;
DOI:10.1021/jf501377t