benzyl 2,3-O-isopropylidene-5-O-trifluoromethylsulphonyl-α-D-lyxofuranoside

Base Information

• Chemical Name: benzyl 2,3-O-isopropylidene-5-O-trifluoromethylsulphonyl-α-D-lyxofuranoside
• CAS No.: 88165-21-3
• Molecular Formula: C₁₆H₁₉F₃O₇S
• Molecular Weight: 412.384

Synonyms:benzyl 2,3-O-isopropylidene-5-O-trifluoromethylsulphonyl-α-D-lyxofuranoside

Chemical Property of benzyl 2,3-O-isopropylidene-5-O-trifluoromethylsulphonyl-α-D-lyxofuranoside

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Technology Process of benzyl 2,3-O-isopropylidene-5-O-trifluoromethylsulphonyl-α-D-lyxofuranoside

There total 1 articles about benzyl 2,3-O-isopropylidene-5-O-trifluoromethylsulphonyl-α-D-lyxofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(6-benzyloxy-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)methanol (20786-73-6) + trifluoromethylsulfonic anhydride (358-23-6) → benzyl 2,3-O-isopropylidene-5-O-trifluoromethylsulphonyl-α-D-lyxofuranoside (88165-21-3)

Guidance literature:

With pyridine; In dichloromethane; at -30 ℃; for 0.5h;

Reference yield: 81.0%

tert-butyl dimethylphosphonoacetate (62327-21-3) + benzyl 2,3-O-isopropylidene-5-O-trifluoromethylsulphonyl-α-D-lyxofuranoside (88165-21-3) → t-butyl (benzyl 5,6-dideoxy-6-dimethoxyphosphoryl-2,3-O-isopropylidene-α-D-lyxo-heptofuranosid)uronate (92591-97-4,92591-98-5)

Guidance literature:

With sodium hydride; 15-crown-5; In N,N-dimethyl-formamide; for 20h; Ambient temperature;

Reference yield: 75.0%

trimethyl phosphonoacetate (5927-18-4) + benzyl 2,3-O-isopropylidene-5-O-trifluoromethylsulphonyl-α-D-lyxofuranoside (88165-21-3) → methyl (benzyl 5,6-dideoxy-6-dimethoxyphosphoryl-2,3-O-isopropylidene-α-D-lyxo-heptofuranosid)uronate (88165-22-4,88165-23-5)

Guidance literature:

With sodium hydride; 18-crown-6 ether; In N,N-dimethyl-formamide; for 16h; Ambient temperature;

upstream raw materials:

(6-benzyloxy-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)methanol

trifluoromethylsulfonic anhydride

Downstream raw materials:

methyl (benzyl 5,6-dideoxy-6-dimethoxyphosphoryl-2,3-O-isopropylidene-α-D-lyxo-heptofuranosid)uronate

t-butyl (benzyl 5,6-dideoxy-6-dimethoxyphosphoryl-2,3-O-isopropylidene-α-D-lyxo-heptofuranosid)uronate

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