4-(methylthio)phenyl methanesulfonate

Base Information

• Chemical Name: 4-(methylthio)phenyl methanesulfonate
• CAS No.: 17067-40-2
• Molecular Formula: C₈H₁₀O₃S₂
• Molecular Weight: 218.298

Synonyms:4-(methylthio)phenyl methanesulfonate

Chemical Property of 4-(methylthio)phenyl methanesulfonate

Chemical Property:

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Technology Process of 4-(methylthio)phenyl methanesulfonate

There total 1 articles about 4-(methylthio)phenyl methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-hydroxythioanisole (1073-72-9) + methanesulfonyl chloride (124-63-0) → 4-(methylthio)phenyl methanesulfonate (17067-40-2)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃; for 15h; Inert atmosphere;

DOI:10.1021/acs.orglett.0c03782

Reference yield: 85.0%

trimethylsilyl cyanide (7677-24-9) + 4-(methylthio)phenyl methanesulfonate (17067-40-2) → 4-thiocyanatophenyl methanesulfonate

Guidance literature:

With Selectfluor; In acetonitrile; at 80 ℃; for 2h; Inert atmosphere;

DOI:10.1021/acs.joc.9b00965

Reference yield: 73.0%

4-(methylthio)phenyl methanesulfonate (17067-40-2) → p-methylsulfonylphenyl methanesulfonate (138373-11-2)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In chloroform; for 120h; Ambient temperature;

upstream raw materials:

4-hydroxythioanisole

methanesulfonyl chloride

Downstream raw materials:

p-methylsulfonylphenyl methanesulfonate

p-chlorophenyl mesylate

methanesulfonic acid 4-chlorosulfonylphenyl ester

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