[5,15-di[((4-ethyl ester)methylene-oxy)phenyl]porphinato]iron(III)-chloride

Base Information

Chemical Name:[5,15-di[((4-ethyl ester)methylene-oxy)phenyl]porphinato]iron(III)-chloride
CAS No.:847567-86-6
Molecular Formula:C₄₀H₃₂ClFeN₄O₆
Molecular Weight:756.017
Hs Code.:

Synonyms:[5,15-di[((4-ethyl ester)methylene-oxy)phenyl]porphinato]iron(III)-chloride

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Chemical Property of [5,15-di[((4-ethyl ester)methylene-oxy)phenyl]porphinato]iron(III)-chloride

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Technology Process of [5,15-di[((4-ethyl ester)methylene-oxy)phenyl]porphinato]iron(III)-chloride

There total 1 articles about [5,15-di[((4-ethyl ester)methylene-oxy)phenyl]porphinato]iron(III)-chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 7647-01-0,15364-23-5
hydrogenchloride

: iron(II) chloride tetrahydrate

: [5,15-di((4-ethyl ester)methylene-oxy)phenyl]porphyrin

: 847567-86-6
[5,15-di[((4-ethyl ester)methylene-oxy)phenyl]porphinato]iron(III)-chloride

Guidance literature:: In ethanol; chloroform; under Ar; porphyrin dissolved in EtOH-CHCl3 with FeCl2*4H2O; refluxed for 2 h; according to T. Ikeue et al.,Inorg. Chem., 2001, 40, 3423; solvent evapd.; chromd. (neutral alumina, THF); dissolved in CHCl3; washed with aq. HCl and H2O; solvent removed;
DOI:10.1021/ja061388m

Reference yield:

: 110-86-1
pyridine

: 847567-86-6
[5,15-di[((4-ethyl ester)methylene-oxy)phenyl]porphinato]iron(III)-chloride

: 909390-94-9
[5,15-di[((4-ethyl ester)methylene-oxy)phenyl]porphinato]iron(III)-(pyridine)2⁽¹⁺⁾

Guidance literature:: In dichloromethane; under N2; pyridine added to soln. of Fe porphyrin in CH2Cl2; not isolated; monitored by UV-vis spectra;
DOI:10.1021/ja061388m