3,4-di-O-benzyl-2-deoxy-6-O-p-methoxyphenyl-2-phthalimido-D-glucopyranose

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Chemical Name:3,4-di-O-benzyl-2-deoxy-6-O-p-methoxyphenyl-2-phthalimido-D-glucopyranose
CAS No.:126713-85-7
Molecular Formula:C₃₅H₃₃NO₈
Molecular Weight:595.649
Hs Code.:

Synonyms:3,4-di-O-benzyl-2-deoxy-6-O-p-methoxyphenyl-2-phthalimido-D-glucopyranose

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Chemical Property of 3,4-di-O-benzyl-2-deoxy-6-O-p-methoxyphenyl-2-phthalimido-D-glucopyranose

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Technology Process of 3,4-di-O-benzyl-2-deoxy-6-O-p-methoxyphenyl-2-phthalimido-D-glucopyranose

There total 6 articles about 3,4-di-O-benzyl-2-deoxy-6-O-p-methoxyphenyl-2-phthalimido-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 126713-84-6
allyl 3,4-di-O-benzyl-2-deoxy-6-O-p-methoxyphenyl-2-phthalimido-β-D-glucopyranoside

: 126713-85-7
2-[(2R,3R,4R,5S,6R)-4,5-Bis-benzyloxy-2-hydroxy-6-(4-methoxy-phenoxymethyl)-tetrahydro-pyran-3-yl]-isoindole-1,3-dione

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; Wilkinson's catalyst; In ethanol; water; benzene;
DOI:10.1016/S0040-4039(01)80741-3

Reference yield:

: 100-39-0
benzyl bromide

: 126713-85-7
2-[(2R,3R,4R,5S,6R)-4,5-Bis-benzyloxy-2-hydroxy-6-(4-methoxy-phenoxymethyl)-tetrahydro-pyran-3-yl]-isoindole-1,3-dione

Guidance literature:: Multi-step reaction with 2 steps

1: Ag₂O/KI / dimethylformamide

2: (Ph₃P)3RhCl/DABCO / ethanol; benzene; H₂O

With 1,4-diaza-bicyclo[2.2.2]octane; Wilkinson's catalyst; potassium iodide; silver(l) oxide; In ethanol; water; N,N-dimethyl-formamide; benzene;
DOI:10.1016/S0040-4039(01)80741-3

Reference yield:

: 125946-67-0
allyl 3-O-benzyl-2-deoxy-6-O-p-methoxyphenyl-2-phthalimido-β-D-glucopyranoside

: 126713-85-7
2-[(2R,3R,4R,5S,6R)-4,5-Bis-benzyloxy-2-hydroxy-6-(4-methoxy-phenoxymethyl)-tetrahydro-pyran-3-yl]-isoindole-1,3-dione

Guidance literature:: Multi-step reaction with 2 steps

1: Ag₂O/KI / dimethylformamide

2: (Ph₃P)3RhCl/DABCO / ethanol; benzene; H₂O

With 1,4-diaza-bicyclo[2.2.2]octane; Wilkinson's catalyst; potassium iodide; silver(l) oxide; In ethanol; water; N,N-dimethyl-formamide; benzene;
DOI:10.1016/S0040-4039(01)80741-3