6-methoxy-2-(4-methoxyphenyl)-3-[4-(2-(piperidin-1-yl)ethylthio)benzoyl]benzo[b]thiophene

Base Information

• Chemical Name: 6-methoxy-2-(4-methoxyphenyl)-3-[4-(2-(piperidin-1-yl)ethylthio)benzoyl]benzo[b]thiophene
• CAS No.: 206434-69-7
• Molecular Formula: C₃₀H₃₁NO₃S₂
• Molecular Weight: 517.713

Synonyms:6-methoxy-2-(4-methoxyphenyl)-3-[4-(2-(piperidin-1-yl)ethylthio)benzoyl]benzo[b]thiophene

Chemical Property of 6-methoxy-2-(4-methoxyphenyl)-3-[4-(2-(piperidin-1-yl)ethylthio)benzoyl]benzo[b]thiophene

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
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Technology Process of 6-methoxy-2-(4-methoxyphenyl)-3-[4-(2-(piperidin-1-yl)ethylthio)benzoyl]benzo[b]thiophene

There total 3 articles about 6-methoxy-2-(4-methoxyphenyl)-3-[4-(2-(piperidin-1-yl)ethylthio)benzoyl]benzo[b]thiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

N-(2-Mercaptoethyl)piperidine (4706-22-3) + 6-methoxy-2-(4-methoxyphenyl)-3-(4-fluorobenzoyl)benzo[b]thiophene (206434-77-7) → 6-methoxy-2-(4-methoxyphenyl)-3-[4-(2-(piperidin-1-yl)ethylthio)benzoyl]benzo[b]thiophene (206434-69-7)

Guidance literature:

With sodium hydride; In diethyl ether; N,N-dimethyl-formamide; at 40 ℃; for 1h;

DOI:10.1016/S0040-4039(98)02533-7

Reference yield:

4-fluorobenzoyl chloride (403-43-0) → 6-methoxy-2-(4-methoxyphenyl)-3-[4-(2-(piperidin-1-yl)ethylthio)benzoyl]benzo[b]thiophene (206434-69-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 74 percent / AlCl₃ / CH₂Cl₂

2: 98 percent / NaH / dimethylformamide; diethyl ether / 1 h / 40 °C

With aluminium trichloride; sodium hydride; In diethyl ether; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1016/S0040-4039(98)02533-7

Reference yield:

2-(4'-methoxyphenyl)-6-methoxybenzothiophene (63675-74-1) → 6-methoxy-2-(4-methoxyphenyl)-3-[4-(2-(piperidin-1-yl)ethylthio)benzoyl]benzo[b]thiophene (206434-69-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 74 percent / AlCl₃ / CH₂Cl₂

2: 98 percent / NaH / dimethylformamide; diethyl ether / 1 h / 40 °C

With aluminium trichloride; sodium hydride; In diethyl ether; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1016/S0040-4039(98)02533-7

upstream raw materials:

N-(2-Mercaptoethyl)piperidine

6-methoxy-2-(4-methoxyphenyl)-3-(4-fluorobenzoyl)benzo[b]thiophene

4-fluorobenzoyl chloride

2-(4'-methoxyphenyl)-6-methoxybenzothiophene

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