methyl 3-O-allyl-2,4,6-tri-O-benzoyl-α-D-mannopyranosyl-(1->3)-2,4,6-tri-O-benzoyl-α-D-mannopyranoside

Base Information

Chemical Name:methyl 3-O-allyl-2,4,6-tri-O-benzoyl-α-D-mannopyranosyl-(1->3)-2,4,6-tri-O-benzoyl-α-D-mannopyranoside
CAS No.:431981-84-9
Molecular Formula:C₅₈H₅₂O₁₇
Molecular Weight:1021.04
Hs Code.:

Synonyms:methyl 3-O-allyl-2,4,6-tri-O-benzoyl-α-D-mannopyranosyl-(1->3)-2,4,6-tri-O-benzoyl-α-D-mannopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 3-O-allyl-2,4,6-tri-O-benzoyl-α-D-mannopyranosyl-(1->3)-2,4,6-tri-O-benzoyl-α-D-mannopyranoside

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Technology Process of methyl 3-O-allyl-2,4,6-tri-O-benzoyl-α-D-mannopyranosyl-(1->3)-2,4,6-tri-O-benzoyl-α-D-mannopyranoside

There total 13 articles about methyl 3-O-allyl-2,4,6-tri-O-benzoyl-α-D-mannopyranosyl-(1->3)-2,4,6-tri-O-benzoyl-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 98-88-4
benzoyl chloride

: 431981-83-8
methyl 3-O-allyl-2,4,6-tri-O-benzoyl-α-D-mannopyranosyl-(1->3)-2-O-benzoyl-α-D-mannopyranoside

: 431981-84-9
methyl 3-O-allyl-2,4,6-tri-O-benzoyl-α-D-mannopyranosyl-(1->3)-2,4,6-tri-O-benzoyl-α-D-mannopyranoside

Guidance literature:: With pyridine; at 20 ℃;
DOI:10.1016/S0008-6215(02)00011-3

Reference yield: 85.0%

: 125226-68-8
methyl 2,4,6-tri-O-benzoyl-α-D-mannopyranoside

: 431981-80-5
3-O-allyl-2,4,6-tri-O-benzoyl-α-D-mannopyranoside trichloroacetimidate

: 431981-84-9
methyl 3-O-allyl-2,4,6-tri-O-benzoyl-α-D-mannopyranosyl-(1->3)-2,4,6-tri-O-benzoyl-α-D-mannopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -25 - 20 ℃; for 3h;
DOI:10.1081/CAR-120014899

Reference yield:

: 125226-68-8
methyl 2,4,6-tri-O-benzoyl-α-D-mannopyranoside

: 3-O-allyl-2,4,6-tri-O-benzoyl-α-D-mannopyranosyl trichloroacetimidate

: 431981-84-9
methyl 3-O-allyl-2,4,6-tri-O-benzoyl-α-D-mannopyranosyl-(1->3)-2,4,6-tri-O-benzoyl-α-D-mannopyranoside

Guidance literature:: methyl 2,4,6-tri-O-benzoyl-α-D-mannopyranoside; 3-O-allyl-2,4,6-tri-O-benzoyl-α-D-mannopyranosyl trichloroacetimidate; With trimethylsilyl trifluoromethanesulfonate; In 1,2-dichloro-ethane; at 0 - 20 ℃; for 0.5h; Molecular sieve;

With triethylamine; In 1,2-dichloro-ethane; at 20 ℃;