Benzoic acid, 3-amino-4-[(methylamino)carbonyl]-, methyl ester (9CI)

Base Information

Chemical Name:Benzoic acid, 3-amino-4-[(methylamino)carbonyl]-, methyl ester (9CI)
CAS No.:183431-11-0
Molecular Formula:C10H12 N2 O3
Molecular Weight:208.21388
Hs Code.:
Mol file:183431-11-0.mol

Synonyms:Benzoic acid, 3-amino-4-[(methylamino)carbonyl]-, methyl ester (9CI)

Suppliers and Price of Benzoic acid, 3-amino-4-[(methylamino)carbonyl]-, methyl ester (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzoic acid, 3-amino-4-[(methylamino)carbonyl]-, methyl ester (9CI)

Chemical Property:

PSA：81.42000
LogP:1.38710

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzoic acid, 3-amino-4-[(methylamino)carbonyl]-, methyl ester (9CI)

There total 5 articles about Benzoic acid, 3-amino-4-[(methylamino)carbonyl]-, methyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 183431-09-6
methyl 4-(methylamino)carbonyl-3-nitrobenzoate

: 183431-11-0
methyl 3-amino-4-(methylamino)carbonylbenzoate

Guidance literature:: With tin(ll) chloride; In ethanol; at 70 ℃; for 1h;
DOI:10.1021/jm970479e

Reference yield:

: 7772-99-8
stannous chloride

: 183431-09-6
methyl 4-(methylamino)carbonyl-3-nitrobenzoate

: 183431-11-0
methyl 3-amino-4-(methylamino)carbonylbenzoate

Guidance literature:: In ethanol;

Reference yield:

: 610-29-7
2-nitroterephthalic acid

: 183431-11-0
methyl 3-amino-4-(methylamino)carbonylbenzoate

Guidance literature:: Multi-step reaction with 4 steps

1: 55 percent / aq. H₂SO₄ / 1 h / Heating

2: SOCl₂, DMF / 3 h / Heating

3: CH₂Cl₂; H₂O / 0.17 h

4: 64 percent / SnCl₂ / ethanol / 1 h / 70 °C

With thionyl chloride; sulfuric acid; N,N-dimethyl-formamide; tin(ll) chloride; In ethanol; dichloromethane; water;
DOI:10.1021/jm970479e