N-benzyloxycarbonyl-L-tyrosyl-D-alanylglycyl-L-phenylalanyl-L-leucine N-methylamine

Base Information

Chemical Name:N-benzyloxycarbonyl-L-tyrosyl-D-alanylglycyl-L-phenylalanyl-L-leucine N-methylamine
CAS No.:83891-97-8
Molecular Formula:C₃₈H₄₈N₆O₈
Molecular Weight:716.835
Hs Code.:

Synonyms:N-benzyloxycarbonyl-L-tyrosyl-D-alanylglycyl-L-phenylalanyl-L-leucine N-methylamine

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Chemical Property of N-benzyloxycarbonyl-L-tyrosyl-D-alanylglycyl-L-phenylalanyl-L-leucine N-methylamine

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Technology Process of N-benzyloxycarbonyl-L-tyrosyl-D-alanylglycyl-L-phenylalanyl-L-leucine N-methylamine

There total 7 articles about N-benzyloxycarbonyl-L-tyrosyl-D-alanylglycyl-L-phenylalanyl-L-leucine N-methylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 83892-16-4
N-benzyloxycarbonyl-L-tyrosyl-D-alanylglycyl-L-phenylalanyl-L-leucine methyl ester

: 74-89-5
methylamine

: 83891-97-8
N-benzyloxycarbonyl-L-tyrosyl-D-alanylglycyl-L-phenylalanyl-L-leucine N-methylamine

Guidance literature:: In methanol; ethanol; for 48h; Ambient temperature;

Reference yield:

: 3850-45-1
Cbz-L-Phe-L-Leu-OMe

: 83891-97-8
N-benzyloxycarbonyl-L-tyrosyl-D-alanylglycyl-L-phenylalanyl-L-leucine N-methylamine

Guidance literature:: Multi-step reaction with 5 steps

1: 76 percent / HBr / acetic acid / 0.75 h

2: 85 percent / N-hydroxybenzotriazole, Et₃N, DCCI / dimethylformamide / 12 h / Ambient temperature

3: H₂ / 10percent Pd/C / methanol / 8 h

4: ethyl acetate / 12 h

5: 72 percent / methanol; ethanol / 48 h / Ambient temperature

With hydrogen bromide; hydrogen; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; ethanol; acetic acid; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 34286-66-3
N-benzyloxycarbonyl-(R)alanyl-glycine

: 83891-97-8
N-benzyloxycarbonyl-L-tyrosyl-D-alanylglycyl-L-phenylalanyl-L-leucine N-methylamine

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / N-hydroxybenzotriazole, Et₃N, DCCI / dimethylformamide / 12 h / Ambient temperature

2: H₂ / 10percent Pd/C / methanol / 8 h

3: ethyl acetate / 12 h

4: 72 percent / methanol; ethanol / 48 h / Ambient temperature

With hydrogen; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; ethanol; ethyl acetate; N,N-dimethyl-formamide;