C₂₇H₂₈N₆O₆S₂

Base Information

Chemical Name:C₂₇H₂₈N₆O₆S₂
CAS No.:1542268-02-9
Molecular Formula:C₂₇H₂₈N₆O₆S₂
Molecular Weight:596.688
Hs Code.:

C<sub>27</sub>H<sub>28</sub>N<sub>6</sub>O<sub>6</sub>S<sub>2</sub>

Synonyms:C₂₇H₂₈N₆O₆S₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₇H₂₈N₆O₆S₂

Chemical Property:

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Technology Process of C₂₇H₂₈N₆O₆S₂

There total 11 articles about C₂₇H₂₈N₆O₆S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1542268-01-8
C₂₇H₂₈N₆O₄S₂

: 1542268-02-9
C₂₇H₂₈N₆O₆S₂

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;

Reference yield:

: 2345-34-8
4-acetyloxy-benzoic acid

: 1542268-02-9
C₂₇H₂₈N₆O₆S₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: oxalyl dichloride / 4 h / 20 °C

2.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 3 h / 20 °C

3.1: potassium carbonate / methanol / 5 h / 20 °C

4.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 1 h / 0 - 4 °C / Inert atmosphere

4.2: 3 h / 20 °C / Inert atmosphere

5.1: bis-triphenylphosphine-palladium(II) chloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 16 h / 90 °C / Inert atmosphere

6.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; oxalyl dichloride; potassium carbonate; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 99-96-7
4-hydroxy-benzoic acid

: 1542268-02-9
C₂₇H₂₈N₆O₆S₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: pyridine / 4 h / 20 °C

2.1: oxalyl dichloride / 4 h / 20 °C

3.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 3 h / 20 °C

4.1: potassium carbonate / methanol / 5 h / 20 °C

5.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 1 h / 0 - 4 °C / Inert atmosphere

5.2: 3 h / 20 °C / Inert atmosphere

6.1: bis-triphenylphosphine-palladium(II) chloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 16 h / 90 °C / Inert atmosphere

7.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C / Inert atmosphere

With pyridine; bis-triphenylphosphine-palladium(II) chloride; oxalyl dichloride; potassium carbonate; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;