11-(2,6-dichlorophenyl)-6-phenyl-6,11-dihydrobenzimidazo[1,2-b]isoquinoline

Base Information

Chemical Name:11-(2,6-dichlorophenyl)-6-phenyl-6,11-dihydrobenzimidazo[1,2-b]isoquinoline
CAS No.:246145-30-2
Molecular Formula:C₂₇H₁₈Cl₂N₂
Molecular Weight:441.359
Hs Code.:

Synonyms:11-(2,6-dichlorophenyl)-6-phenyl-6,11-dihydrobenzimidazo[1,2-b]isoquinoline

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Chemical Property of 11-(2,6-dichlorophenyl)-6-phenyl-6,11-dihydrobenzimidazo[1,2-b]isoquinoline

Chemical Property:

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Technology Process of 11-(2,6-dichlorophenyl)-6-phenyl-6,11-dihydrobenzimidazo[1,2-b]isoquinoline

There total 3 articles about 11-(2,6-dichlorophenyl)-6-phenyl-6,11-dihydrobenzimidazo[1,2-b]isoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 525-06-4
diphenyl ketene

: 1042161-51-2
(2-Azido-phenyl)-[1-(2,6-dichloro-phenyl)-meth-(E)-ylidene]-amine

: 246145-30-2
11-(2,6-dichlorophenyl)-6-phenyl-6,11-dihydrobenzimidazo[1,2-b]isoquinoline

Guidance literature:: (2-Azido-phenyl)-[1-(2,6-dichloro-phenyl)-meth-(E)-ylidene]-amine; With trimethylphosphane; In toluene; at 20 ℃; for 0.166667h;

diphenyl ketene; In toluene; at 20 ℃; for 0.5h;
DOI:10.1016/S0040-4039(99)01222-8

Reference yield:

: 1005-07-8
o-azidoaniline

: 246145-30-2
11-(2,6-dichlorophenyl)-6-phenyl-6,11-dihydrobenzimidazo[1,2-b]isoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1.1: AcOH / ethanol / 0.5 h / Heating

2.1: trimethylphosphane 1M / toluene / 0.17 h / 20 °C

2.2: toluene / 0.5 h / 20 °C

With acetic acid; trimethylphosphane; In ethanol; toluene; 1.1: Condensation / 2.1: Substitution / 2.2: Substitution;
DOI:10.1016/S0040-4039(99)01222-8

Reference yield:

: 83-38-5
2,6-dichlorobenzaldehyde

: 246145-30-2
11-(2,6-dichlorophenyl)-6-phenyl-6,11-dihydrobenzimidazo[1,2-b]isoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1.1: AcOH / ethanol / 0.5 h / Heating

2.1: trimethylphosphane 1M / toluene / 0.17 h / 20 °C

2.2: toluene / 0.5 h / 20 °C

With acetic acid; trimethylphosphane; In ethanol; toluene; 1.1: Condensation / 2.1: Substitution / 2.2: Substitution;
DOI:10.1016/S0040-4039(99)01222-8