ethyl 2-((5-(3-(methoxycarbonyl)phenyl)furan-2-yl)methylene)-3-oxo-5,7-diphenyl-3,5-dihydro-2H-thiazolo[3,2-a]pyrimidine-6-carboxylate

Base Information

Chemical Name:ethyl 2-((5-(3-(methoxycarbonyl)phenyl)furan-2-yl)methylene)-3-oxo-5,7-diphenyl-3,5-dihydro-2H-thiazolo[3,2-a]pyrimidine-6-carboxylate
CAS No.:306984-71-4
Molecular Formula:C₃₄H₂₆N₂O₆S
Molecular Weight:590.656
Hs Code.:

Synonyms:ethyl 2-((5-(3-(methoxycarbonyl)phenyl)furan-2-yl)methylene)-3-oxo-5,7-diphenyl-3,5-dihydro-2H-thiazolo[3,2-a]pyrimidine-6-carboxylate

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Chemical Property of ethyl 2-((5-(3-(methoxycarbonyl)phenyl)furan-2-yl)methylene)-3-oxo-5,7-diphenyl-3,5-dihydro-2H-thiazolo[3,2-a]pyrimidine-6-carboxylate

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Technology Process of ethyl 2-((5-(3-(methoxycarbonyl)phenyl)furan-2-yl)methylene)-3-oxo-5,7-diphenyl-3,5-dihydro-2H-thiazolo[3,2-a]pyrimidine-6-carboxylate

There total 4 articles about ethyl 2-((5-(3-(methoxycarbonyl)phenyl)furan-2-yl)methylene)-3-oxo-5,7-diphenyl-3,5-dihydro-2H-thiazolo[3,2-a]pyrimidine-6-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 591723-69-2
methyl 3-(5-formylfuran-2-yl)benzoate

: C₂₁H₂₀N₂O₃S

: 306984-71-4
ethyl 2-((5-(3-(methoxycarbonyl)phenyl)furan-2-yl)methylene)-3-oxo-5,7-diphenyl-3,5-dihydro-2H-thiazolo[3,2-a]pyrimidine-6-carboxylate

Guidance literature:: With acetic acid; 3-amino propanoic acid; at 100 ℃; for 1h;
DOI:10.1016/j.ejmech.2010.12.014

Reference yield:

: 94-02-0
ethyl 3-oxo-3-phenylpropionate

: 306984-71-4
ethyl 2-((5-(3-(methoxycarbonyl)phenyl)furan-2-yl)methylene)-3-oxo-5,7-diphenyl-3,5-dihydro-2H-thiazolo[3,2-a]pyrimidine-6-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: stannous chloride dihydrate / ethanol / Reflux

2: sodium acetate; acetic anhydride / Reflux

3: acetic acid; 3-amino propanoic acid / 1 h / 100 °C

With stannous chloride dihydrate; sodium acetate; acetic anhydride; acetic acid; 3-amino propanoic acid; In ethanol; 1: Biginelli pyrimidine synthesis;
DOI:10.1016/j.ejmech.2010.12.014

Reference yield:

: 100-52-7
benzaldehyde

: 306984-71-4
ethyl 2-((5-(3-(methoxycarbonyl)phenyl)furan-2-yl)methylene)-3-oxo-5,7-diphenyl-3,5-dihydro-2H-thiazolo[3,2-a]pyrimidine-6-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: stannous chloride dihydrate / ethanol / Reflux

2: sodium acetate; acetic anhydride / Reflux

3: acetic acid; 3-amino propanoic acid / 1 h / 100 °C

With stannous chloride dihydrate; sodium acetate; acetic anhydride; acetic acid; 3-amino propanoic acid; In ethanol; 1: Biginelli pyrimidine synthesis;
DOI:10.1016/j.ejmech.2010.12.014