Phenyl 2-azido-2-deoxy-3,4,6-tri-O-benzyl-1-seleno-α-D-mannopyranoside

Base Information

Chemical Name:Phenyl 2-azido-2-deoxy-3,4,6-tri-O-benzyl-1-seleno-α-D-mannopyranoside
CAS No.:150809-71-5
Molecular Formula:C₃₃H₃₃N₃O₄Se
Molecular Weight:614.603
Hs Code.:

Synonyms:Phenyl 2-azido-2-deoxy-3,4,6-tri-O-benzyl-1-seleno-α-D-mannopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Phenyl 2-azido-2-deoxy-3,4,6-tri-O-benzyl-1-seleno-α-D-mannopyranoside

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Technology Process of Phenyl 2-azido-2-deoxy-3,4,6-tri-O-benzyl-1-seleno-α-D-mannopyranoside

There total 2 articles about Phenyl 2-azido-2-deoxy-3,4,6-tri-O-benzyl-1-seleno-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 55628-54-1
3,4,6-tri-O-benzyl-D-glucal

: 1666-13-3
diphenyl diselenide

: 150809-71-5
Phenyl 2-azido-2-deoxy-3,4,6-tri-O-benzyl-1-seleno-α-D-mannopyranoside

: 150809-70-4
Phenyl 2-azido-2-deoxy-3,4,6-tri-O-benzyl-1-seleno-α-D-glucopyranoside

Guidance literature:: With sodium azide; [bis(acetoxy)iodo]benzene; In dichloromethane; for 96h; Ambient temperature;
DOI:10.1021/jo00074a048

Reference yield:

: 71098-88-9
N-phenylselanylphthalimide

: 55628-54-1
3,4,6-tri-O-benzyl-D-glucal

: 150809-71-5
Phenyl 2-azido-2-deoxy-3,4,6-tri-O-benzyl-1-seleno-α-D-mannopyranoside

: 150809-70-4
Phenyl 2-azido-2-deoxy-3,4,6-tri-O-benzyl-1-seleno-α-D-glucopyranoside

Guidance literature:: With trimethylsilylazide; tetrabutyl ammonium fluoride; In dichloromethane; Yield given. Yields of byproduct given;
DOI:10.1039/c39940000035

Reference yield:

: 150809-71-5
Phenyl 2-azido-2-deoxy-3,4,6-tri-O-benzyl-1-seleno-α-D-mannopyranoside

: (2R,3S,4R,5S,6R)-4,5-Bis-benzyloxy-6-benzyloxymethyl-2-phenylselanyl-tetrahydro-pyran-3-ylamine

Guidance literature:: With 1.3-propanedithiol; sodium tetrahydroborate; triethylamine; In isopropyl alcohol; at 45 ℃; for 4h;
DOI:10.1080/07328309608005438