(S_p)-butylmethylphenylphoshine oxide

Base Information

Chemical Name:(S_p)-butylmethylphenylphoshine oxide
CAS No.:55794-15-5
Molecular Formula:C₁₁H₁₇OP
Molecular Weight:196.229
Hs Code.:

(S<SUB>p</SUB>)-butylmethylphenylphoshine oxide

Synonyms:(S_p)-butylmethylphenylphoshine oxide

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Chemical Property of (S_p)-butylmethylphenylphoshine oxide

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Technology Process of (S_p)-butylmethylphenylphoshine oxide

There total 13 articles about (S_p)-butylmethylphenylphoshine oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 109-72-8,29786-93-4
n-butyllithium

: 1164367-99-0
(-)-menthyl phenylphosphinate

: 74-88-4
methyl iodide

: 55794-15-5
(S_p)-butylmethylphenylphoshine oxide

Guidance literature:: n-butyllithium; (-)-menthyl phenylphosphinate; In hexane; pentane; at -80 ℃;

methyl iodide; In hexane; pentane; at 0 ℃;

Reference yield: 84.0%

: 109-72-8,29786-93-4
n-butyllithium

: 31352-60-0,31352-61-1,54353-18-3
(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl phenylphosphinate

: 74-88-4
methyl iodide

: 55794-15-5
(S_p)-butylmethylphenylphoshine oxide

Guidance literature:: n-butyllithium; (1R,2S,5R)-2-isopropyl-5-methylcyclohexyl phenylphosphinate; In hexane; at -80 ℃; for 7h; Inert atmosphere;

methyl iodide; In hexane; at 0 ℃; for 24h; optical yield given as %ee; Inert atmosphere;
DOI:10.1021/ja804412k

Reference yield: 60.0%

: 693-03-8
n-butyl magnesium bromide

: 7301-81-7,34638-79-4,33642-98-7
ethyl (S)-methyl(phenyl)phosphinate

: 55794-15-5
(S_p)-butylmethylphenylphoshine oxide

Guidance literature:: In tetrahydrofuran; at 20 ℃; for 12h; enantioselective reaction; Schlenk technique; Inert atmosphere;
DOI:10.1039/d1cc00646k