(4R,2E)-4-hydroxy-4-[(1S,6R)-6-isopropyl-3-methyl-2-oxocyclohex-3-enyl]-3-methylbut-2-enyl acetate

Base Information

Chemical Name:(4R,2E)-4-hydroxy-4-[(1S,6R)-6-isopropyl-3-methyl-2-oxocyclohex-3-enyl]-3-methylbut-2-enyl acetate
CAS No.:1207372-45-9
Molecular Formula:C₁₇H₂₆O₄
Molecular Weight:294.391
Hs Code.:

Synonyms:(4R,2E)-4-hydroxy-4-[(1S,6R)-6-isopropyl-3-methyl-2-oxocyclohex-3-enyl]-3-methylbut-2-enyl acetate

Suppliers and Price of (4R,2E)-4-hydroxy-4-[(1S,6R)-6-isopropyl-3-methyl-2-oxocyclohex-3-enyl]-3-methylbut-2-enyl acetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (4R,2E)-4-hydroxy-4-[(1S,6R)-6-isopropyl-3-methyl-2-oxocyclohex-3-enyl]-3-methylbut-2-enyl acetate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (4R,2E)-4-hydroxy-4-[(1S,6R)-6-isopropyl-3-methyl-2-oxocyclohex-3-enyl]-3-methylbut-2-enyl acetate

There total 1 articles about (4R,2E)-4-hydroxy-4-[(1S,6R)-6-isopropyl-3-methyl-2-oxocyclohex-3-enyl]-3-methylbut-2-enyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 26586-02-7
(E)-4-acetoxy-2-methylcrotonaldehyde

: 499-71-8
carvotanacetone

: 1207372-66-4
(4S,2E)-4-hydroxy-4-[(1S,6R)-6-isopropyl-3-methyl-2-oxocyclohex-3-enyl]-3-methylbut-2-enyl acetate

: 1207372-45-9
(4R,2E)-4-hydroxy-4-[(1S,6R)-6-isopropyl-3-methyl-2-oxocyclohex-3-enyl]-3-methylbut-2-enyl acetate

Guidance literature:: carvotanacetone; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 0.75h; Inert atmosphere;

(E)-4-acetoxy-2-methylcrotonaldehyde; In tetrahydrofuran; at -78 ℃; for 3h; optical yield given as %de; Inert atmosphere;
DOI:10.1055/s-0029-1216990

Reference yield: 93.0%

: 1207372-45-9
(4R,2E)-4-hydroxy-4-[(1S,6R)-6-isopropyl-3-methyl-2-oxocyclohex-3-enyl]-3-methylbut-2-enyl acetate

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1207372-69-7
C₂₃H₄₀O₄Si

Guidance literature:: (4R,2E)-4-hydroxy-4-[(1S,6R)-6-isopropyl-3-methyl-2-oxocyclohex-3-enyl]-3-methylbut-2-enyl acetate; With 1H-imidazole; In N,N-dimethyl-formamide; for 0.166667h;

tert-butyldimethylsilyl chloride; In N,N-dimethyl-formamide; at 20 ℃; for 16h;
DOI:10.1055/s-0029-1216990