Technology Process of 4-(aminothioxomethyl)-N-(2,5-dimethylphenyl)-1-piperidinecarboxamide
There total 3 articles about 4-(aminothioxomethyl)-N-(2,5-dimethylphenyl)-1-piperidinecarboxamide which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium hydrogen sulfide monohydrate; diethyl amine hydrochloride;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 72h;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: diethyl ether / 0.5 h / 0 °C
2: diethyl amine hydrochloride; sodium hydrogen sulfide monohydrate / N,N-dimethyl-formamide / 72 h / 20 °C
With
sodium hydrogen sulfide monohydrate; diethyl amine hydrochloride;
In
diethyl ether; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: diethyl ether / 0.5 h / 0 °C
2: diethyl amine hydrochloride; sodium hydrogen sulfide monohydrate / N,N-dimethyl-formamide / 72 h / 20 °C
With
sodium hydrogen sulfide monohydrate; diethyl amine hydrochloride;
In
diethyl ether; N,N-dimethyl-formamide;