dimethyl 6,7-methylenedioxy-(3',4'-dimethoxyphenyl)naphthalene-2,3-dicarboxylate

Base Information

Chemical Name:dimethyl 6,7-methylenedioxy-(3',4'-dimethoxyphenyl)naphthalene-2,3-dicarboxylate
CAS No.:66130-46-9
Molecular Formula:C₂₃H₂₀O₈
Molecular Weight:424.407
Hs Code.:

Synonyms:dimethyl 6,7-methylenedioxy-(3',4'-dimethoxyphenyl)naphthalene-2,3-dicarboxylate

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Chemical Property of dimethyl 6,7-methylenedioxy-(3',4'-dimethoxyphenyl)naphthalene-2,3-dicarboxylate

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Technology Process of dimethyl 6,7-methylenedioxy-(3',4'-dimethoxyphenyl)naphthalene-2,3-dicarboxylate

There total 8 articles about dimethyl 6,7-methylenedioxy-(3',4'-dimethoxyphenyl)naphthalene-2,3-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: C₁₆H₁₈O₆

: 717903-52-1
6-(trimethylsilyl)benzo[d][1,3]dioxol-5-yl triflate

: 66130-46-9
dimethyl 6,7-methylenedioxy-(3',4'-dimethoxyphenyl)naphthalene-2,3-dicarboxylate

Guidance literature:: With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; cesium fluoride; 1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazolium chloride; In acetonitrile; at 60 ℃; for 24h; Inert atmosphere; Reflux;
DOI:10.1021/ol3028658

Reference yield: 53.0%

: 2788-26-3
dimethyl 2-(dimethoxyphosphoryl)succinate

: 473253-65-5
3,4-dimethoxybenzyl-(6-formylbenzo[1,3]dioxol-5-yl)methanone

: 66130-46-9
dimethyl 6,7-methylenedioxy-(3',4'-dimethoxyphenyl)naphthalene-2,3-dicarboxylate

Guidance literature:: With sodium methylate; In tetrahydrofuran; methanol; at 0 ℃; for 3h;
DOI:10.1016/S0040-4020(02)00616-6

Reference yield:

: dimethyl 5-(((trifluoromethyl)sulfonyl)oxy) naphtha[2,3-d][1,3]dioxole-6,7-dicarboxylate

: 122775-35-3
3,4-Dimethoxyphenylboronic acid

: 66130-46-9
dimethyl 6,7-methylenedioxy-(3',4'-dimethoxyphenyl)naphthalene-2,3-dicarboxylate

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium fluoride; In 1,4-dioxane; at 90 ℃; Inert atmosphere;
DOI:10.2174/1573406416666200610190417