α-piperonylidene-β-veratralidenesuccinic anhydride

Base Information

Chemical Name:α-piperonylidene-β-veratralidenesuccinic anhydride
CAS No.:42923-54-6
Molecular Formula:C₂₁H₁₆O₇
Molecular Weight:380.354
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of α-piperonylidene-β-veratralidenesuccinic anhydride

Chemical Property:

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Technology Process of α-piperonylidene-β-veratralidenesuccinic anhydride

There total 1 articles about α-piperonylidene-β-veratralidenesuccinic anhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 42923-54-6
β-(3,4-Dimethoxy-benzyliden)-α-(3,4-methylendioxy-benzyliden)-succinanhydrid

Guidance literature:: C21H18O8, Acetylchlorid, Siedehitze;
DOI:10.1039/jr9630002983

Reference yield:

: 42923-54-6,53945-02-1,91364-75-9
α-piperonylidene-β-veratralidenesuccinic anhydride

: 17951-19-8
justicidin B

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) DDQ, HCl gas, 2.) LiAlH₄ / 1.) benzene, reflux, 8 h, 2.) THF, reflux, 6h

2: 6 mg / silica gel - silver carbonate / benzene / 3 h / Heating

With hydrogenchloride; lithium aluminium tetrahydride; silica gel; silver carbonate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In benzene;

Reference yield:

: 42923-54-6,53945-02-1,91364-75-9
α-piperonylidene-β-veratralidenesuccinic anhydride

: 5707-96-0
retrochinensin

Guidance literature:: Multi-step reaction with 3 steps

2: 220 mg / LiAlH₄ / tetrahydrofuran / 6 h / Heating

3: 58 mg / silica gel - silver carbonate / benzene / 3 h / Heating

With lithium aluminium tetrahydride; silica gel; silver carbonate; In tetrahydrofuran; benzene;