(3R,4R,5S)-4-acetamido-5-[(tert-butoxycarbonyl)-amino]-3-(1-ethylpropoxy)-1-bromocyclohexene

Base Information

Chemical Name:(3R,4R,5S)-4-acetamido-5-[(tert-butoxycarbonyl)-amino]-3-(1-ethylpropoxy)-1-bromocyclohexene
CAS No.:1062100-84-8
Molecular Formula:C₁₈H₃₁BrN₂O₄
Molecular Weight:419.359
Hs Code.:

Synonyms:(3R,4R,5S)-4-acetamido-5-[(tert-butoxycarbonyl)-amino]-3-(1-ethylpropoxy)-1-bromocyclohexene

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Chemical Property of (3R,4R,5S)-4-acetamido-5-[(tert-butoxycarbonyl)-amino]-3-(1-ethylpropoxy)-1-bromocyclohexene

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Technology Process of (3R,4R,5S)-4-acetamido-5-[(tert-butoxycarbonyl)-amino]-3-(1-ethylpropoxy)-1-bromocyclohexene

There total 9 articles about (3R,4R,5S)-4-acetamido-5-[(tert-butoxycarbonyl)-amino]-3-(1-ethylpropoxy)-1-bromocyclohexene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 764639-63-6
(3R,4R,5S)-4-acetamido-5-[(tert-butoxycarbonyl)-amino]-3-(1-ethylpropoxy)-1-cyclohexene-1-carboxylic acid

: 1062100-84-8
(3R,4R,5S)-4-acetamido-5-[(tert-butoxycarbonyl)-amino]-3-(1-ethylpropoxy)-1-bromocyclohexene

Guidance literature:: (3R,4R,5S)-4-acetamido-5-[(tert-butoxycarbonyl)-amino]-3-(1-ethylpropoxy)-1-cyclohexene-1-carboxylic acid; With dmap; triethylamine; S-(1-oxido-2-pyridyl)-thio-N,N,N',N'-tetramethyluronium hexafluorophosphate; In tetrahydrofuran;

With Bromotrichloromethane; In dichloromethane; Irradiation;
DOI:10.1042/BCJ20180764

Reference yield: 78.0%

: 1122581-40-1
N-[(1R,2R,6R)-4-bromo-2-(1-ethylpropoxy)-6-hydroxycyclohex-3-en-1-yl]acetamide

: 39139-87-2
tetrabutylammonium isocyanate

: 75-65-0
tert-butyl alcohol

: 1062100-84-8
(3R,4R,5S)-4-acetamido-5-[(tert-butoxycarbonyl)-amino]-3-(1-ethylpropoxy)-1-bromocyclohexene

Guidance literature:: N-[(1R,2R,6R)-4-bromo-2-(1-ethylpropoxy)-6-hydroxycyclohex-3-en-1-yl]acetamide; tetrabutylammonium isocyanate; With triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In acetonitrile; at 20 ℃; for 18h;

tert-butyl alcohol; In acetonitrile; for 24h; Heating / reflux;

Reference yield: 76.0%

: 1373702-86-3
C₂₃H₃₅N₃O₆S₂

: 1062100-84-8
(3R,4R,5S)-4-acetamido-5-[(tert-butoxycarbonyl)-amino]-3-(1-ethylpropoxy)-1-bromocyclohexene

Guidance literature:: With 2,2'-azobis(isobutyronitrile); Bromotrichloromethane; at 70 ℃; for 1h; Inert atmosphere;
DOI:10.1055/s-0031-1290356