H-ILKEPVHGY-SCH₂CH₂CO₂H

Base Information

Chemical Name:H-ILKEPVHGY-SCH₂CH₂CO₂H
CAS No.:1271876-09-5
Molecular Formula:C₅₃H₈₂N₁₂O₁₄S
Molecular Weight:1143.37
Hs Code.:

H-ILKEPVHGY-SCH<SUB>2</SUB>CH<SUB>2</SUB>CO<SUB>2</SUB>H

Synonyms:H-ILKEPVHGY-SCH₂CH₂CO₂H

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of H-ILKEPVHGY-SCH₂CH₂CO₂H

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Technology Process of H-ILKEPVHGY-SCH₂CH₂CO₂H

There total 3 articles about H-ILKEPVHGY-SCH₂CH₂CO₂H which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1255709-32-0
C₅₄H₈₅N₁₃O₁₂S₂

: 107-96-0
3-mercaptopropionic acid

: 1271876-09-5
C₅₃H₈₂N₁₂O₁₄S

Guidance literature:: With tris-(2-carboxyethyl)-phosphine hydrochloride; sodium hydroxide; In water; at 37 ℃; for 16h; pH=4; aq. phosphate buffer; Inert atmosphere;
DOI:10.1021/jo200029e

Reference yield: 53.0%

: 1255709-32-0
C₅₄H₈₅N₁₃O₁₂S₂

: C₅H₉NO₃S

: 107-96-0
3-mercaptopropionic acid

: 1271876-09-5
H-ILKEPVHGY-SCH₂CH₂CO₂H

Guidance literature:: With 4-mercaptophenylacetic acid; guanidine hydrochloride; tris-(2-carboxyethyl)-phosphine hydrochloride; sodium hydroxide; In aq. phosphate buffer; at 37 ℃; for 48h; pH=7; Inert atmosphere; Glovebox;
DOI:10.1039/c6ob01079b

Reference yield:

: 1255709-49-9
C₅₄H₈₇N₁₃O₁₂S₂

: 1271876-09-5
C₅₃H₈₂N₁₂O₁₄S

Guidance literature:: Multi-step reaction with 2 steps

1: oxygen; ammonium bicarbonate / pH 8

2: tris-(2-carboxyethyl)-phosphine hydrochloride; sodium hydroxide / water / 16 h / 37 °C / pH 4 / aq. phosphate buffer; Inert atmosphere

With oxygen; tris-(2-carboxyethyl)-phosphine hydrochloride; ammonium bicarbonate; sodium hydroxide; In water;
DOI:10.1021/jo200029e