1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3,4,5-tridodecyloxybenzene

Base Information

Chemical Name:1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3,4,5-tridodecyloxybenzene
CAS No.:1329426-07-4
Molecular Formula:C₄₈H₈₉BO₅
Molecular Weight:757.043
Hs Code.:

Synonyms:1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3,4,5-tridodecyloxybenzene

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Chemical Property of 1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3,4,5-tridodecyloxybenzene

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Technology Process of 1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3,4,5-tridodecyloxybenzene

There total 5 articles about 1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3,4,5-tridodecyloxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 73183-34-3
bis(pinacol)diborane

: 654065-52-8
1-bromo-3,4,5-tris-n-dodecyloxybenzene

: 1329426-07-4
1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3,4,5-tridodecyloxybenzene

Guidance literature:: With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; In dimethyl sulfoxide; at 85 ℃; for 24h; Inert atmosphere;
DOI:10.1021/acs.inorgchem.8b02984

Reference yield: 60.0%

: 61676-62-8
2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 654065-52-8
1-bromo-3,4,5-tris-n-dodecyloxybenzene

: 1329426-07-4
1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3,4,5-tridodecyloxybenzene

Guidance literature:: 1-bromo-3,4,5-tris-n-dodecyloxybenzene; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 1h; Inert atmosphere;

2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane; In tetrahydrofuran; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1021/ja3001979

Reference yield: 2.39%

: 5-bromo-1,2,3-tris(octyloxy)benzene

: 73183-34-3
bis(pinacol)diborane

: 1329426-07-4
1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3,4,5-tridodecyloxybenzene

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; potassium acetate; In 1,4-dioxane; at 80 ℃; for 48h; Inert atmosphere;
DOI:10.1002/chem.201300993