3-(4-((2',6'-dimethyl-[1,1'-biphenyl]-3-yl)methoxy)phenyl)propiolic acid

Base Information

Chemical Name:3-(4-((2',6'-dimethyl-[1,1'-biphenyl]-3-yl)methoxy)phenyl)propiolic acid
CAS No.:1312788-44-5
Molecular Formula:C₂₄H₂₀O₃
Molecular Weight:356.421
Hs Code.:

Synonyms:3-(4-((2',6'-dimethyl-[1,1'-biphenyl]-3-yl)methoxy)phenyl)propiolic acid

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Chemical Property of 3-(4-((2',6'-dimethyl-[1,1'-biphenyl]-3-yl)methoxy)phenyl)propiolic acid

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Technology Process of 3-(4-((2',6'-dimethyl-[1,1'-biphenyl]-3-yl)methoxy)phenyl)propiolic acid

There total 8 articles about 3-(4-((2',6'-dimethyl-[1,1'-biphenyl]-3-yl)methoxy)phenyl)propiolic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₅H₂₂Br₂O₃

: 1312788-44-5
3-(4-((2',6'-dimethyl-[1,1'-biphenyl]-3-yl)methoxy)phenyl)propiolic acid

Guidance literature:: With potassium hydroxide; In isopropyl alcohol; at 90 ℃; for 6h; Inert atmosphere;
DOI:10.1016/j.ejmech.2018.08.075

Reference yield:

: C₂₆H₂₄O₃

: 1312788-44-5
3-(4-((2',6'-dimethyl-[1,1'-biphenyl]-3-yl)methoxy)phenyl)propiolic acid

Guidance literature:: C₂₆H₂₄O₃; With lithium hydroxide monohydrate; water; In methanol; for 6h; Reflux;

With hydrogenchloride; In methanol; water;

Reference yield:

: 1312788-55-8
3'-(chloromethyl)-2,6-dimethyl-1,1'-biphenyl

: 1312788-44-5
3-(4-((2',6'-dimethyl-[1,1'-biphenyl]-3-yl)methoxy)phenyl)propiolic acid

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 20 °C

2: lithium hydroxide monohydrate; water / methanol / 6 h / Reflux

With lithium hydroxide monohydrate; water; potassium carbonate; potassium iodide; In methanol; N,N-dimethyl-formamide;