allyl 4-O-benzyl-6-O-<6-O-benzyloxymethyl-3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-β-D-glucopyranosyl>-3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-β-D-glucopyranoside 4'-...

Base Information

• Chemical Name: allyl 4-O-benzyl-6-O-<6-O-benzyloxymethyl-3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-β-D-glucopyranosyl>-3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-β-D-glucopyranoside 4'-...
• CAS No.: 92949-61-6
• Molecular Formula: C₁₂₆H₁₇₉N₂O₂₁P
• Molecular Weight: 2088.78

Synonyms:allyl 4-O-benzyl-6-O-<6-O-benzyloxymethyl-3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-β-D-glucopyranosyl>-3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-β-D-glucopyranoside 4'-...

Chemical Property of allyl 4-O-benzyl-6-O-<6-O-benzyloxymethyl-3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-β-D-glucopyranosyl>-3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-β-D-glucopyranoside 4'-...

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Technology Process of allyl 4-O-benzyl-6-O-<6-O-benzyloxymethyl-3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-β-D-glucopyranosyl>-3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-β-D-glucopyranoside 4'-...

There total 2 articles about allyl 4-O-benzyl-6-O-<6-O-benzyloxymethyl-3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-β-D-glucopyranosyl>-3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-β-D-glucopyranoside 4'-... which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

allyl 4-O-benzyl-6-O-<6-O-benzyloxymethyl-3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-β-D-glucopyranosyl>-3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-β-D-glucopyranoside (92949-59-2) + chlorophosphoric acid diphenyl ester (2524-64-3) → allyl 4-O-benzyl-6-O-<6-O-benzyloxymethyl-3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-β-D-glucopyranosyl>-3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-β-D-glucopyranoside 4'-... (92949-61-6)

Guidance literature:

With pyridine; dmap; In dichloromethane; for 7h; Ambient temperature;

DOI:10.1016/S0040-4039(01)81258-2

Reference yield:

C84H115N2O17P + (R)-3-benzyloxytetradecanoic acid (87357-67-3) → allyl 4-O-benzyl-6-O-<6-O-benzyloxymethyl-3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-β-D-glucopyranosyl>-3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-β-D-glucopyranoside 4'-... (92949-61-6)

Guidance literature:

With dicyclohexyl-carbodiimide; dmap; In dichloromethane; Yield given; Ambient temperature;

DOI:10.1016/S0040-4039(00)84384-1

Reference yield:

allyl 4-O-benzyl-6-O-<6-O-benzyloxymethyl-3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-β-D-glucopyranosyl>-3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-β-D-glucopyranoside 4'-... (92949-61-6) → 4-O-benzyl-6-O-<6-O-benzyloxymethyl-3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-β-D-glucopyranosyl>-3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-D-glucopyranose 4'-diphenyl ph...

Guidance literature:

With (1,5-cyclooctadiene)bis(methyldiphenylphosphine) iridium hexafluorophosphate; iodine; Yield given. Multistep reaction;

DOI:10.1016/S0040-4039(01)81258-2

upstream raw materials:

(R)-3-benzyloxytetradecanoic acid

allyl 4-O-benzyl-6-O-<6-O-benzyloxymethyl-3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-β-D-glucopyranosyl>-3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-β-D-glucopyranoside

chlorophosphoric acid diphenyl ester

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