4-(3,5-dimethylpyridin-4-yl)-N-(diphenylmethylene)-3,5-dimethyl-benzenamine

Base Information

Chemical Name:4-(3,5-dimethylpyridin-4-yl)-N-(diphenylmethylene)-3,5-dimethyl-benzenamine
CAS No.:865087-48-5
Molecular Formula:C₂₈H₂₆N₂
Molecular Weight:390.528
Hs Code.:

Synonyms:4-(3,5-dimethylpyridin-4-yl)-N-(diphenylmethylene)-3,5-dimethyl-benzenamine

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Chemical Property of 4-(3,5-dimethylpyridin-4-yl)-N-(diphenylmethylene)-3,5-dimethyl-benzenamine

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Technology Process of 4-(3,5-dimethylpyridin-4-yl)-N-(diphenylmethylene)-3,5-dimethyl-benzenamine

There total 8 articles about 4-(3,5-dimethylpyridin-4-yl)-N-(diphenylmethylene)-3,5-dimethyl-benzenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.7%

: 865087-54-3
trifluoromethane sulfonic acid 4-(3,5-dimethyl-pyridin-4-yl)-3,5-dimethyl-phenyl ester

: 1013-88-3
Benzophenone imine

: 865087-48-5
4-(3,5-dimethylpyridin-4-yl)-N-(diphenylmethylene)-3,5-dimethyl-benzenamine

Guidance literature:: With caesium carbonate; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In tetrahydrofuran; at 65 ℃; for 15h;
DOI:10.1021/ol051365x

Reference yield:

: 865087-45-2
4-(4-methoxy-2,6-dimethylphenyl)-3,5-dimethyl-pyridine

: 865087-48-5
4-(3,5-dimethylpyridin-4-yl)-N-(diphenylmethylene)-3,5-dimethyl-benzenamine

Guidance literature:: Multi-step reaction with 3 steps

1: 91.6 percent / pyridine*HCl / 3 h / 210 °C

2: 92.8 percent / pyridine / 6 h / 20 °C

3: 97.7 percent / Cs₂CO₃; BINAP / Pd(OAc)2 / tetrahydrofuran / 15 h / 65 °C

With pyridine; pyridine hydrochloride; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; palladium diacetate; In tetrahydrofuran;
DOI:10.1021/ja0674690

Reference yield:

: 865087-46-3
4-(3,5-dimethylpyridin-4-yl)-3,5-dimethyl-phenol

: 865087-48-5
4-(3,5-dimethylpyridin-4-yl)-N-(diphenylmethylene)-3,5-dimethyl-benzenamine

Guidance literature:: Multi-step reaction with 2 steps

1: 92.8 percent / pyridine / 6 h / 20 °C

2: 97.7 percent / Cs₂CO₃; BINAP / Pd(OAc)2 / tetrahydrofuran / 15 h / 65 °C

With pyridine; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; palladium diacetate; In tetrahydrofuran;
DOI:10.1021/ja0674690