(1R,2R,3S,4R,5S)-phenyl-2,3,4,6-tetra-O-(trimethylsilyl)-β-D-glucopyranoside

Base Information

Chemical Name:(1R,2R,3S,4R,5S)-phenyl-2,3,4,6-tetra-O-(trimethylsilyl)-β-D-glucopyranoside
CAS No.:120788-25-2
Molecular Formula:C₂₄H₄₈O₆Si₄
Molecular Weight:544.984
Hs Code.:

Synonyms:(1R,2R,3S,4R,5S)-phenyl-2,3,4,6-tetra-O-(trimethylsilyl)-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,2R,3S,4R,5S)-phenyl-2,3,4,6-tetra-O-(trimethylsilyl)-β-D-glucopyranoside

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Technology Process of (1R,2R,3S,4R,5S)-phenyl-2,3,4,6-tetra-O-(trimethylsilyl)-β-D-glucopyranoside

There total 4 articles about (1R,2R,3S,4R,5S)-phenyl-2,3,4,6-tetra-O-(trimethylsilyl)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 27607-77-8
trimethylsilyl trifluoromethanesulfonate

: 1464-44-4
phenyl-β-D-glucopyranoside

: 120788-25-2
(1R,2R,3S,4R,5S)-phenyl-2,3,4,6-tetra-O-(trimethylsilyl)-β-D-glucopyranoside

Guidance literature:: With 1,1,1,3,3,3-hexamethyl-disilazane; In dichloromethane; at 25 ℃;
DOI:10.1002/anie.201708109

Reference yield:

: 999-97-3
1,1,1,3,3,3-hexamethyl-disilazane

: 1464-44-4
phenyl-β-D-glucopyranoside

: 120788-25-2
(1R,2R,3S,4R,5S)-phenyl-2,3,4,6-tetra-O-(trimethylsilyl)-β-D-glucopyranoside

Guidance literature:: With trifluoroacetic acid; at 45 ℃; for 0.5h;
DOI:10.1016/j.foodchem.2010.10.097

Reference yield:

: 604-69-3
β-D-glucose pentaacetate

: 120788-25-2
(1R,2R,3S,4R,5S)-phenyl-2,3,4,6-tetra-O-(trimethylsilyl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: boron trifluoride diethyl etherate / dichloromethane / 18 h / 25 °C

1.2: 12 h / 25 °C

2.1: 1,1,1,3,3,3-hexamethyl-disilazane / dichloromethane / 25 °C

With boron trifluoride diethyl etherate; 1,1,1,3,3,3-hexamethyl-disilazane; In dichloromethane;
DOI:10.1002/anie.201708109