ethyl (2R,3S)-3-(biphenyl-4-ylcarbonyl)-1-(4-methoxyphenyl)aziridine-2-carboxylate

Base Information

Chemical Name:ethyl (2R,3S)-3-(biphenyl-4-ylcarbonyl)-1-(4-methoxyphenyl)aziridine-2-carboxylate
CAS No.:1153714-89-6
Molecular Formula:C₂₅H₂₃NO₄
Molecular Weight:401.462
Hs Code.:

Synonyms:ethyl (2R,3S)-3-(biphenyl-4-ylcarbonyl)-1-(4-methoxyphenyl)aziridine-2-carboxylate

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Chemical Property of ethyl (2R,3S)-3-(biphenyl-4-ylcarbonyl)-1-(4-methoxyphenyl)aziridine-2-carboxylate

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Technology Process of ethyl (2R,3S)-3-(biphenyl-4-ylcarbonyl)-1-(4-methoxyphenyl)aziridine-2-carboxylate

There total 1 articles about ethyl (2R,3S)-3-(biphenyl-4-ylcarbonyl)-1-(4-methoxyphenyl)aziridine-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 623-73-4
diazoacetic acid ethyl ester

: 1145-04-6
2-([1,1'-biphenyl]-4-yl)-2-oxoacetaldehyde monohydrate

: 104-94-9
4-methoxy-aniline

: 1153714-89-6
ethyl (2R,3S)-3-(biphenyl-4-ylcarbonyl)-1-(4-methoxyphenyl)aziridine-2-carboxylate

Guidance literature:: 2-([1,1'-biphenyl]-4-yl)-2-oxoacetaldehyde monohydrate; 4-methoxy-aniline; With (R)-3,3'-bis(tris(4-tert-butylphenyl)silyl)-1,1'-binaphthyl-2,2'-diyl hydrogenphosphate; In toluene; at 20 ℃; for 1h;

diazoacetic acid ethyl ester; In toluene; at -30 ℃; for 23h; optical yield given as %ee; enantioselective reaction;
DOI:10.1021/ol900674t