2-[3-(Trifluoromethyl)phenyl]ethanethioamide, 3-(2-Amino-2-thioxoethyl)benzotrifluoride

Base Information

• Chemical Name: 2-[3-(Trifluoromethyl)phenyl]ethanethioamide, 3-(2-Amino-2-thioxoethyl)benzotrifluoride
• CAS No.: 952182-78-4
• Molecular Formula: C₉H₈F₃NS
• Molecular Weight: 219.23
• Hs Code.: 2934208090
• Mol file: 952182-78-4.mol

Synonyms:2-(3-(trifluoromethyl)phenyl)ethanethioamide

Chemical Property of 2-[3-(Trifluoromethyl)phenyl]ethanethioamide, 3-(2-Amino-2-thioxoethyl)benzotrifluoride

Chemical Property:

• Melting Point: 78～80℃

Purity/Quality:

98%min ^*data from raw suppliers

2-[3-(Trifluoromethyl)phenyl]ethanethioamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of 2-[3-(Trifluoromethyl)phenyl]ethanethioamide, 3-(2-Amino-2-thioxoethyl)benzotrifluoride

There total 1 articles about 2-[3-(Trifluoromethyl)phenyl]ethanethioamide, 3-(2-Amino-2-thioxoethyl)benzotrifluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

3-trifluoromethylphenylacetonitrile (2338-76-3) → 2-(3-(trifluoromethyl)phenyl)ethanethioamide (952182-78-4)

Guidance literature:

With hydrogenchloride; O,O-Diethyl hydrogen phosphorodithioate; In ethyl acetate; at 20 ℃; Product distribution / selectivity;

Reference yield: 97.0%

2-(3-(trifluoromethyl)phenyl)ethanethioamide (952182-78-4) + 1-bromoacetone (598-31-2) → 4-methyl-2-(3-(trifluoromethyl)benzyl)-1,3-thiazole

Guidance literature:

In ethanol; for 2h; Reflux;

DOI:10.1016/j.bmc.2017.03.064

Reference yield: 93.0%

2-(3-(trifluoromethyl)phenyl)ethanethioamide (952182-78-4) + ethyl 2-chloro-3-oxo-butyrate (609-15-4) → ethyl 4-methyl-2-[3-(trifluoromethyl)benzyl]-1,3-thiazole-5-carboxylate (959708-64-6)

Guidance literature:

With pyridine; at 20 ℃; for 7h; Product distribution / selectivity;

upstream raw materials:

3-trifluoromethylphenylacetonitrile

Downstream raw materials:

2-[3-(trifluoromethyl)benzyl]-1,3-thiazole-5-carboxylic acid

4-methyl-2-[3-(trifluoromethyl)benzyl]-1,3-thiazole-5-carboxylic acid

1-methyl-N-{4-(trifluoromethyl)-2-[3-(trifluoromethyl)benzyl]-1,3-thiazol-5-yl}-1H-pyrazole-5-carboxamide

4-(trifluoromethyl)-2-[3-(trifluoromethyl)benzyl]-1,3-thiazole-5-carboxylic acid

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