2-Nitro-4-iodo-5-fluorotoluene

Base Information Edit

Chemical Name:2-Nitro-4-iodo-5-fluorotoluene
CAS No.:259860-34-9
Molecular Formula:C₇H₅FINO₂
Molecular Weight:281.025
Hs Code.:2902900000
Mol file:259860-34-9.mol

Synonyms:1-fluoro-2-iodo-5-methyl-4-nitro-benzene

Suppliers and Price of 2-Nitro-4-iodo-5-fluorotoluene

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
1-Fluoro-2-iodo-5-methyl-4-nitrobenzene 95+%
1g
$ 475.00

Total 2 raw suppliers

Chemical Property of 2-Nitro-4-iodo-5-fluorotoluene Edit

Chemical Property:

Melting Point:46.5-47.5 °C
Boiling Point:293.8±35.0 °C(Predicted)
Density:1.953±0.06 g/cm3(Predicted)

Purity/Quality:

99% ^*data from raw suppliers

1-Fluoro-2-iodo-5-methyl-4-nitrobenzene 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-Nitro-4-iodo-5-fluorotoluene

There total 2 articles about 2-Nitro-4-iodo-5-fluorotoluene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 259860-00-9
2-fluoro-4-methyl-5-nitro-phenylamine

: 259860-34-9
1-fluoro-2-iodo-5-methyl-4-nitro-benzene

Guidance literature:: 2-fluoro-4-methyl-5-nitro-phenylamine; With hydrogenchloride; In water; at 0 ℃;

With sodium nitrite; In water; at -10 ℃; for 0.666667h;

With potassium iodide; In water; at 0 - 20 ℃; for 2h;

Reference yield:

: 452-80-2
2-fluoro-4-methylaniline

: 259860-34-9
1-fluoro-2-iodo-5-methyl-4-nitro-benzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: 94 percent / HNO₃; H₂SO₄ / -10 °C

2.1: NaNO₂; aq. HCl / 0 °C

2.2: KI / H₂O

With hydrogenchloride; sulfuric acid; nitric acid; sodium nitrite;
DOI:10.1016/j.bmcl.2003.05.001