5-<5-Benzyloxycarbonyl-3-(2-methoxycarbonylethyl)-4-methoxycarbonylmethylpyrrol-2-ylmethyl>-5-<5-<5-formyl-4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethylpyrrol-2-ylmethyl>-4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethylpyrrol-2-ylmethyl>pyrrolidi

Base Information

• Chemical Name: 5-<5-Benzyloxycarbonyl-3-(2-methoxycarbonylethyl)-4-methoxycarbonylmethylpyrrol-2-ylmethyl>-5-<5-<5-formyl-4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethylpyrrol-2-ylmethyl>-4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethylpyrrol-2-ylmethyl>pyrrolidi
• CAS No.: 101210-45-1
• Molecular Formula: C₄₉H₅₈N₄O₁₆
• Molecular Weight: 959.017

Synonyms:5-<5-Benzyloxycarbonyl-3-(2-methoxycarbonylethyl)-4-methoxycarbonylmethylpyrrol-2-ylmethyl>-5-<5-<5-formyl-4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethylpyrrol-2-ylmethyl>-4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethylpyrrol-2-ylmethyl>pyrrolidi

Chemical Property of 5-<5-Benzyloxycarbonyl-3-(2-methoxycarbonylethyl)-4-methoxycarbonylmethylpyrrol-2-ylmethyl>-5-<5-<5-formyl-4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethylpyrrol-2-ylmethyl>-4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethylpyrrol-2-ylmethyl>pyrrolidi

Chemical Property:

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99% ，98% ^*data from raw suppliers

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Technology Process of 5-<5-Benzyloxycarbonyl-3-(2-methoxycarbonylethyl)-4-methoxycarbonylmethylpyrrol-2-ylmethyl>-5-<5-<5-formyl-4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethylpyrrol-2-ylmethyl>-4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethylpyrrol-2-ylmethyl>pyrrolidi

There total 12 articles about 5-<5-Benzyloxycarbonyl-3-(2-methoxycarbonylethyl)-4-methoxycarbonylmethylpyrrol-2-ylmethyl>-5-<5-<5-formyl-4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethylpyrrol-2-ylmethyl>-4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethylpyrrol-2-ylmethyl>pyrrolidi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

3-(5-acetoxymethyl-2-formyl-4-methoxycarbonylmethyl-pyrrol-3-yl)-propionic acid methyl ester (58950-46-2) + 5-<5-Benzyloxycarbonyl-3-(2-methoxycarbonylethyl)-4-methoxycarbonylmethylpyrrol-2-ylmethyl>-5-<4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethylpyrrol-2-ylmethyl>pyrrolidin-2-one (101210-44-0) → 5-<5-Benzyloxycarbonyl-3-(2-methoxycarbonylethyl)-4-methoxycarbonylmethylpyrrol-2-ylmethyl>-5-<5-<5-formyl-4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethylpyrrol-2-ylmethyl>-4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethylpyrrol-2-ylmethyl>pyrrolidi (101210-45-1)

Guidance literature:

With tin(IV) chloride; In tetrahydrofuran; dichloromethane; for 15.5h; Ambient temperature;

Reference yield:

Benzyl 4-(2-Methoxycarbonylethyl)-3-methoxycarbonylmethyl-5-(2-nitroethyl)pyrrole-2-carboxylate (101210-39-3) → 5-<5-Benzyloxycarbonyl-3-(2-methoxycarbonylethyl)-4-methoxycarbonylmethylpyrrol-2-ylmethyl>-5-<5-<5-formyl-4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethylpyrrol-2-ylmethyl>-4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethylpyrrol-2-ylmethyl>pyrrolidi (101210-45-1)

Guidance literature:

Multi-step reaction with 6 steps

1: methylamine / acetic acid

2: borohydride

3: 1.) Triton B

4: Zn / acetic acid

6: tin(IV) chloride / CH₂Cl₂

With borohydride; N-benzyl-trimethylammonium hydroxide; methylamine; zinc; tin(IV) chloride; In dichloromethane; acetic acid;

DOI:10.1039/c39850001294

Reference yield:

1-3-<4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethyl-5-t-butoxycarbonylpyrrol-2-yl>-2-nitropropane (101231-96-3) → 5-<5-Benzyloxycarbonyl-3-(2-methoxycarbonylethyl)-4-methoxycarbonylmethylpyrrol-2-ylmethyl>-5-<5-<5-formyl-4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethylpyrrol-2-ylmethyl>-4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethylpyrrol-2-ylmethyl>pyrrolidi (101210-45-1)

Guidance literature:

Multi-step reaction with 4 steps

1: 1.) Triton B

2: Zn / acetic acid

4: tin(IV) chloride / CH₂Cl₂

With N-benzyl-trimethylammonium hydroxide; zinc; tin(IV) chloride; In dichloromethane; acetic acid;

DOI:10.1039/c39850001294

upstream raw materials:

3-(5-acetoxymethyl-2-formyl-4-methoxycarbonylmethyl-pyrrol-3-yl)-propionic acid methyl ester

5-<5-Benzyloxycarbonyl-3-(2-methoxycarbonylethyl)-4-methoxycarbonylmethylpyrrol-2-ylmethyl>-5-<4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethylpyrrol-2-ylmethyl>pyrrolidin-2-one

Benzyl 4-(2-Methoxycarbonylethyl)-3-methoxycarbonylmethyl-5-(2-nitroethyl)pyrrole-2-carboxylate

1-3-<4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethyl-5-t-butoxycarbonylpyrrol-2-yl>-2-nitropropane

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