methyl 3-[3-[5-benzyloxy-2-ethyl-4-(4-fluorophenyl)phenoxy]propoxy]-2-propylbenzoate

Base Information

Chemical Name:methyl 3-[3-[5-benzyloxy-2-ethyl-4-(4-fluorophenyl)phenoxy]propoxy]-2-propylbenzoate
CAS No.:1447666-96-7
Molecular Formula:C₃₅H₃₇FO₅
Molecular Weight:556.674
Hs Code.:

Synonyms:methyl 3-[3-[5-benzyloxy-2-ethyl-4-(4-fluorophenyl)phenoxy]propoxy]-2-propylbenzoate

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Chemical Property of methyl 3-[3-[5-benzyloxy-2-ethyl-4-(4-fluorophenyl)phenoxy]propoxy]-2-propylbenzoate

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Technology Process of methyl 3-[3-[5-benzyloxy-2-ethyl-4-(4-fluorophenyl)phenoxy]propoxy]-2-propylbenzoate

There total 6 articles about methyl 3-[3-[5-benzyloxy-2-ethyl-4-(4-fluorophenyl)phenoxy]propoxy]-2-propylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 152120-07-5
2-benzyloxy-1-(4-fluorophenyl)-5-ethyl-4-(3-chloro-1-propyloxy)benzene

: 183108-35-2
methyl 3-hydroxy-2-n-propylbenzoate

: 1447666-96-7
methyl 3-[3-[5-benzyloxy-2-ethyl-4-(4-fluorophenyl)phenoxy]propoxy]-2-propylbenzoate

Guidance literature:: With dmap; potassium carbonate; In dimethyl sulfoxide; at 60 ℃; for 87h;

Reference yield:

: 1409654-45-0
tert-butyl 2,3-dimethoxybenzoate

: 1447666-96-7
methyl 3-[3-[5-benzyloxy-2-ethyl-4-(4-fluorophenyl)phenoxy]propoxy]-2-propylbenzoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: acetic acid / tetrahydrofuran; diethyl ether / 3.5 h / -12 - -10 °C

2.1: boron tribromide / toluene / 3 h / -25 - -5 °C

2.2: 0.5 h / 7 °C

3.1: thionyl chloride / 35.5 h / -10 °C

4.1: potassium carbonate; dmap / dimethyl sulfoxide / 87 h / 60 °C

With dmap; thionyl chloride; boron tribromide; potassium carbonate; acetic acid; In tetrahydrofuran; diethyl ether; dimethyl sulfoxide; toluene;

Reference yield:

: 1521-38-6
2,3-dimethoxybenzoic acid

: 1447666-96-7
methyl 3-[3-[5-benzyloxy-2-ethyl-4-(4-fluorophenyl)phenoxy]propoxy]-2-propylbenzoate

Guidance literature:: Multi-step reaction with 6 steps

1.1: N,N-dimethyl-formamide; thionyl chloride / toluene / 1 h / 40 °C

2.1: pyridine; dmap / dichloromethane / 1.08 h / Reflux

3.1: acetic acid / tetrahydrofuran; diethyl ether / 3.5 h / -12 - -10 °C

4.1: boron tribromide / toluene / 3 h / -25 - -5 °C

4.2: 0.5 h / 7 °C

5.1: thionyl chloride / 35.5 h / -10 °C

6.1: potassium carbonate; dmap / dimethyl sulfoxide / 87 h / 60 °C

With pyridine; dmap; thionyl chloride; boron tribromide; potassium carbonate; acetic acid; N,N-dimethyl-formamide; In tetrahydrofuran; diethyl ether; dichloromethane; dimethyl sulfoxide; toluene;