7-(2-(tert-butyldiphenylsilyl)ethoxy)-8-(3-methylbut-2-en-1-yl)-2H-chromen-2-one

Base Information

Chemical Name:7-(2-(tert-butyldiphenylsilyl)ethoxy)-8-(3-methylbut-2-en-1-yl)-2H-chromen-2-one
CAS No.:1161258-91-8
Molecular Formula:C₃₂H₃₆O₃Si
Molecular Weight:496.722
Hs Code.:

Synonyms:7-(2-(tert-butyldiphenylsilyl)ethoxy)-8-(3-methylbut-2-en-1-yl)-2H-chromen-2-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7-(2-(tert-butyldiphenylsilyl)ethoxy)-8-(3-methylbut-2-en-1-yl)-2H-chromen-2-one

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Technology Process of 7-(2-(tert-butyldiphenylsilyl)ethoxy)-8-(3-methylbut-2-en-1-yl)-2H-chromen-2-one

There total 1 articles about 7-(2-(tert-butyldiphenylsilyl)ethoxy)-8-(3-methylbut-2-en-1-yl)-2H-chromen-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 173440-20-5
2-(tert-butyldiphenylsilyl)ethanol

: 484-14-0
osthenol

: 1161258-91-8
7-(2-(tert-butyldiphenylsilyl)ethoxy)-8-(3-methylbut-2-en-1-yl)-2H-chromen-2-one

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/jo900613u

Reference yield:

: 1161258-91-8
7-(2-(tert-butyldiphenylsilyl)ethoxy)-8-(3-methylbut-2-en-1-yl)-2H-chromen-2-one

: 3804-70-4
columbianetin

: 52842-47-4
(R)-8-(2-hydroxypropan-2-yl)-8,9-dihydro-2H-furo[2,3-h]chromen-2-one

Guidance literature:: 7-(2-(tert-butyldiphenylsilyl)ethoxy)-8-(3-methylbut-2-en-1-yl)-2H-chromen-2-one; With borax; Oxone; Shi's ketone; water; edetate disodium; potassium carbonate; tetrabutylammonium sulfate; In Dimethoxymethane; acetonitrile; at 20 ℃; Inert atmosphere;

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 50 ℃; for 16h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1021/jo900613u