(p-(dimethylamino)phenyl)mercuric chloride

Base Information

• Chemical Name: (p-(dimethylamino)phenyl)mercuric chloride
• CAS No.: 23000-67-1
• Molecular Formula: C₈H₁₀HgN*Cl
• Molecular Weight: 356.217
• Mol file: 23000-67-1.mol

Synonyms:(p-(dimethylamino)phenyl)mercuric chloride

Chemical Property of (p-(dimethylamino)phenyl)mercuric chloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (p-(dimethylamino)phenyl)mercuric chloride

There total 3 articles about (p-(dimethylamino)phenyl)mercuric chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

p-dimethylaminophenylmercury acetate (23332-31-2) + lithium chloride → (p-(CH3)2N-C6H4)HgCl (23000-67-1)

Guidance literature:

In water; acetone; Hg-contg. compd. was dissolved in hot acetone and treated with excess ofsatd. aq. soln. of LiCl; stirring for a few minutes; the complex was collected by filtration and air-dried; elem. anal.;

DOI:10.1016/j.jorganchem.2003.10.040

Reference yield:

(p-(dimethylamino)phenyl)mercuric acetate (23332-31-2) + sodium chloride (7647-14-5) → (p-(dimethylamino)phenyl)mercuric chloride (23000-67-1)

Guidance literature:

In water; shaked with aq. NaCl; extd. with diethyl ether, dried over MgSO4,, evapd.;

DOI:10.1021/ja00402a017

Reference yield:

N,N-dimethyl-aniline (121-69-7,77733-26-7) → (p-(CH3)2N-C6H4)HgCl (23000-67-1)

Guidance literature:

Multi-step reaction with 2 steps

1: ethanol

2: water; acetone

In ethanol; water; acetone;

DOI:10.1016/j.jorganchem.2003.10.040

upstream raw materials:

p-dimethylaminophenylmercury acetate

N,N-dimethyl-aniline

(p-(dimethylamino)phenyl)mercuric acetate

sodium chloride

Downstream raw materials:

Cl₂BC₆H₄-4-N(CH₃)2

4-(CH₃)2NC₆H₄BClN(CH₃)(CH₂C₆H₅)