Trimethyl-(1-{2-[3-((1S,5S)-1-methyl-2-oxo-5-vinyl-cyclopentyl)-1-trimethylsilanyl-propyl]-phenyl}-ethyl)-ammonium; iodide

Base Information

Chemical Name:Trimethyl-(1-{2-[3-((1S,5S)-1-methyl-2-oxo-5-vinyl-cyclopentyl)-1-trimethylsilanyl-propyl]-phenyl}-ethyl)-ammonium; iodide
CAS No.:76463-53-1
Molecular Formula:C₂₅H₄₂NOSi*I
Molecular Weight:527.605
Hs Code.:

Synonyms:Trimethyl-(1-{2-[3-((1S,5S)-1-methyl-2-oxo-5-vinyl-cyclopentyl)-1-trimethylsilanyl-propyl]-phenyl}-ethyl)-ammonium; iodide

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Chemical Property of Trimethyl-(1-{2-[3-((1S,5S)-1-methyl-2-oxo-5-vinyl-cyclopentyl)-1-trimethylsilanyl-propyl]-phenyl}-ethyl)-ammonium; iodide

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Technology Process of Trimethyl-(1-{2-[3-((1S,5S)-1-methyl-2-oxo-5-vinyl-cyclopentyl)-1-trimethylsilanyl-propyl]-phenyl}-ethyl)-ammonium; iodide

There total 21 articles about Trimethyl-(1-{2-[3-((1S,5S)-1-methyl-2-oxo-5-vinyl-cyclopentyl)-1-trimethylsilanyl-propyl]-phenyl}-ethyl)-ammonium; iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 42142-24-5
<α-(o-methylphenyl)ethyl>dimethylamine

: 76463-53-1
Trimethyl-(1-{2-[3-((1S,5S)-1-methyl-2-oxo-5-vinyl-cyclopentyl)-1-trimethylsilanyl-propyl]-phenyl}-ethyl)-ammonium; iodide

Guidance literature:: Multi-step reaction with 3 steps

2: HClO₄ / tetrahydrofuran; H₂O / 2 h / Ambient temperature

With perchloric acid; In tetrahydrofuran; water;
DOI:10.1021/ja00390a036

Reference yield:

: 83781-91-3
2-((1R,2R)-1,8,8-Trimethyl-2-vinyl-6,10-dioxa-spiro[4.5]dec-1-yl)-ethanol

: 76463-53-1
Trimethyl-(1-{2-[3-((1S,5S)-1-methyl-2-oxo-5-vinyl-cyclopentyl)-1-trimethylsilanyl-propyl]-phenyl}-ethyl)-ammonium; iodide

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine / 5 h / 0 °C

2: LiBr*H₂O / dimethylformamide / 48 h / Ambient temperature

4: HClO₄ / tetrahydrofuran; H₂O / 2 h / Ambient temperature

With pyridine; perchloric acid; lithium bromide; In tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1021/ja00390a036

Reference yield:

: 76463-45-1,86284-20-0,114673-86-8
trans-2-(β-bromoethyl)-2-methyl-3-vinylcyclopentanone 2,2-dimethylpropanediol ketal

: 76463-53-1
Trimethyl-(1-{2-[3-((1S,5S)-1-methyl-2-oxo-5-vinyl-cyclopentyl)-1-trimethylsilanyl-propyl]-phenyl}-ethyl)-ammonium; iodide

Guidance literature:: Multi-step reaction with 3 steps

2: HClO₄ / tetrahydrofuran; H₂O / 2 h / Ambient temperature

With perchloric acid; In tetrahydrofuran; water;
DOI:10.1021/ja00390a036