1-(2'-deoxy-5'-O-4,4'-dimethoxytrityl-β-D-erythro-ribofuranosyl)-2-selenothymine

Base Information

Chemical Name:1-(2'-deoxy-5'-O-4,4'-dimethoxytrityl-β-D-erythro-ribofuranosyl)-2-selenothymine
CAS No.:1213779-13-5
Molecular Formula:C₃₁H₃₂N₂O₆Se
Molecular Weight:607.565
Hs Code.:

Synonyms:1-(2'-deoxy-5'-O-4,4'-dimethoxytrityl-β-D-erythro-ribofuranosyl)-2-selenothymine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(2'-deoxy-5'-O-4,4'-dimethoxytrityl-β-D-erythro-ribofuranosyl)-2-selenothymine

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Technology Process of 1-(2'-deoxy-5'-O-4,4'-dimethoxytrityl-β-D-erythro-ribofuranosyl)-2-selenothymine

There total 3 articles about 1-(2'-deoxy-5'-O-4,4'-dimethoxytrityl-β-D-erythro-ribofuranosyl)-2-selenothymine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1213779-12-4
1-(2'-deoxy-5'-O-4,4'-dimethoxytrityl-β-D-erythro-ribofuranosyl)-2-methylthiothymine

: 1213779-13-5
1-(2'-deoxy-5'-O-4,4'-dimethoxytrityl-β-D-erythro-ribofuranosyl)-2-selenothymine

Guidance literature:: With selenium; sodium tetrahydroborate; In ethanol; Inert atmosphere;
DOI:10.1039/d0cc07922g

Reference yield: 83.0%

: C₃₂H₃₆N₂O₆S

: 1213779-13-5
1-(2'-deoxy-5'-O-4,4'-dimethoxytrityl-β-D-erythro-ribofuranosyl)-2-selenothymine

Guidance literature:: With selenium; sodium tetrahydroborate; In ethanol; at 0 ℃; Inert atmosphere;

Reference yield:

: 125258-60-8
1-((2R,4S,5R)-5-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-4-hydroxytetrahydrofuran-2-yl)-5-methyl-2-thioxo-2,3-dihydropyrimidin-4(1H)-one

: 1213779-13-5
1-(2'-deoxy-5'-O-4,4'-dimethoxytrityl-β-D-erythro-ribofuranosyl)-2-selenothymine

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane; toluene / 1 h / 20 °C

2: selenium; sodium tetrahydroborate / ethanol / 0 °C / Inert atmosphere

With selenium; sodium tetrahydroborate; N-ethyl-N,N-diisopropylamine; In ethanol; dichloromethane; toluene;