methyl 4-benzyloxy-3-(2'-hydroxy-4'-methoxy-6'-propylbenzoyloxy)-6-hydroxy-2-pentylbenzoate

Base Information

Chemical Name:methyl 4-benzyloxy-3-(2'-hydroxy-4'-methoxy-6'-propylbenzoyloxy)-6-hydroxy-2-pentylbenzoate
CAS No.:113487-80-2
Molecular Formula:C₃₁H₃₆O₈
Molecular Weight:536.622
Hs Code.:

Synonyms:methyl 4-benzyloxy-3-(2'-hydroxy-4'-methoxy-6'-propylbenzoyloxy)-6-hydroxy-2-pentylbenzoate

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Chemical Property of methyl 4-benzyloxy-3-(2'-hydroxy-4'-methoxy-6'-propylbenzoyloxy)-6-hydroxy-2-pentylbenzoate

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Technology Process of methyl 4-benzyloxy-3-(2'-hydroxy-4'-methoxy-6'-propylbenzoyloxy)-6-hydroxy-2-pentylbenzoate

There total 4 articles about methyl 4-benzyloxy-3-(2'-hydroxy-4'-methoxy-6'-propylbenzoyloxy)-6-hydroxy-2-pentylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 6245-56-3
2-hydroxy-4-methoxy-6-propylbenzoic acid

: 113487-78-8
methyl 4-benzyloxy-2,5-dihydroxy-6-pentylbenzoate

: 113487-80-2
methyl 4-benzyloxy-3-(2'-hydroxy-4'-methoxy-6'-propylbenzoyloxy)-6-hydroxy-2-pentylbenzoate

Guidance literature:: With trifluoroacetic anhydride; In toluene; for 2h; Ambient temperature;
DOI:10.1071/CH9871451

Reference yield:

: 58016-28-7
methyl 2,6-dihydroxy-6-pentylbenzoate

: 113487-80-2
methyl 4-benzyloxy-3-(2'-hydroxy-4'-methoxy-6'-propylbenzoyloxy)-6-hydroxy-2-pentylbenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 43 percent / potassium carbonate / acetone / 22 h / Heating

2: 19 percent / potassium persulfate, 20percent sodium hydroxide, dimethyl sulfoxide / 24 h / 10 - 20 °C

3: 76 percent / trifluofoacetic anhydride / toluene / 2 h / Ambient temperature

With sodium hydroxide; potassium peroxomonosulphate; potassium carbonate; dimethyl sulfoxide; trifluoroacetic anhydride; In acetone; toluene;
DOI:10.1071/CH9871451

Reference yield:

: 100-39-0
benzyl bromide

: 113487-80-2
methyl 4-benzyloxy-3-(2'-hydroxy-4'-methoxy-6'-propylbenzoyloxy)-6-hydroxy-2-pentylbenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 43 percent / potassium carbonate / acetone / 22 h / Heating

2: 19 percent / potassium persulfate, 20percent sodium hydroxide, dimethyl sulfoxide / 24 h / 10 - 20 °C

3: 76 percent / trifluofoacetic anhydride / toluene / 2 h / Ambient temperature

With sodium hydroxide; potassium peroxomonosulphate; potassium carbonate; dimethyl sulfoxide; trifluoroacetic anhydride; In acetone; toluene;
DOI:10.1071/CH9871451