p-carbomethoxyphenyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranoside

Base Information

Chemical Name:p-carbomethoxyphenyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranoside
CAS No.:135608-50-3
Molecular Formula:C₂₂H₂₇NO₁₁
Molecular Weight:481.456
Hs Code.:

Synonyms:p-carbomethoxyphenyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranoside

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Chemical Property of p-carbomethoxyphenyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranoside

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Technology Process of p-carbomethoxyphenyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranoside

There total 4 articles about p-carbomethoxyphenyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 99-76-3,156291-94-0
methyl 4-hydroxylbenzoate

: 3068-34-6
Acetic acid (2R,3S,4R,5R,6R)-3-acetoxy-2-acetoxymethyl-5-acetylamino-6-chloro-tetrahydro-pyran-4-yl ester

: 135608-50-3
p-carbomethoxyphenyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: With 15-crown-5; potassium carbonate; In acetonitrile; at 20 ℃; for 17.5h;
DOI:10.1023/A:1012988719296

Reference yield: 55.0%

: 67-56-1
methanol

: 70622-68-3
4-formylphenyl 3,4,6-tri-O-acetyl-2-(acetamido)-2-deoxy-β-D-glucopyranoside

: 135608-50-3
p-carbomethoxyphenyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: With bromine; sodium hydrogencarbonate; for 1.5h; Ambient temperature;

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 135608-50-3
p-carbomethoxyphenyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / tetrabutylammonium hydrogen sulfate, 1M NaOH / CH₂Cl₂ / 0.75 h / Ambient temperature

2: 55 percent / Br₂, NaHCO₃ / 1.5 h / Ambient temperature

With sodium hydroxide; bromine; tetra(n-butyl)ammonium hydrogensulfate; sodium hydrogencarbonate; In dichloromethane;