N-(tert-butyloxycarbonyl)amino-ethane-sulfonyl-phenylalanine-methylester

Base Information

Chemical Name:N-(tert-butyloxycarbonyl)amino-ethane-sulfonyl-phenylalanine-methylester
CAS No.:148200-69-5
Molecular Formula:C₁₇H₂₆N₂O₆S
Molecular Weight:386.469
Hs Code.:

Synonyms:N-(tert-butyloxycarbonyl)amino-ethane-sulfonyl-phenylalanine-methylester

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Chemical Property of N-(tert-butyloxycarbonyl)amino-ethane-sulfonyl-phenylalanine-methylester

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Technology Process of N-(tert-butyloxycarbonyl)amino-ethane-sulfonyl-phenylalanine-methylester

There total 5 articles about N-(tert-butyloxycarbonyl)amino-ethane-sulfonyl-phenylalanine-methylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 24424-99-5
di-tert-butyl dicarbonate

: Tau-Phe-OMe*HBr

: 148200-69-5
N-(tert-butyloxycarbonyl)amino-ethane-sulfonyl-phenylalanine-methylester

Guidance literature:: With TEA; In 1,4-dioxane; at 20 ℃;
DOI:10.1016/j.farmac.2004.07.014

Reference yield:

: (S)-2-(2-tert-Butoxycarbonylamino-ethanesulfinylamino)-3-phenyl-propionic acid methyl ester

: 148200-69-5
N-(tert-butyloxycarbonyl)amino-ethane-sulfonyl-phenylalanine-methylester

Guidance literature:: With sodium periodate; ruthenium trichloride; In dichloromethane; water; acetonitrile; at 0 ℃; Yield given;
DOI:10.1016/S0040-4020(01)86293-1

Reference yield:

: 67385-10-8
di-tert-butyl(disulfanediylbis(ethane-2,1-diyl))dicarbamate

: 148200-69-5
N-(tert-butyloxycarbonyl)amino-ethane-sulfonyl-phenylalanine-methylester

Guidance literature:: Multi-step reaction with 3 steps

1: Cl₂, Ac₂O / CH₂Cl₂ / 1 h / -18 °C

2: N-methylmorpholine / CH₂Cl₂; dimethylformamide / Ambient temperature

3: NaIO₄ / RuCl₃*H₂O / CH₂Cl₂; acetonitrile; H₂O / 0 °C

With 4-methyl-morpholine; sodium periodate; acetic anhydride; chlorine; ruthenium trichloride; In dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0040-4020(01)86293-1