3-(Bis(methylthio)methyl)-1-(4-chlorophenylsulfonyl)-2,3-dihydroquinolin-4(1H)-one

Base Information

Chemical Name:3-(Bis(methylthio)methyl)-1-(4-chlorophenylsulfonyl)-2,3-dihydroquinolin-4(1H)-one
CAS No.:959996-88-4
Molecular Formula:C₁₈H₁₈ClNO₃S₃
Molecular Weight:427.997
Hs Code.:

Synonyms:3-(Bis(methylthio)methyl)-1-(4-chlorophenylsulfonyl)-2,3-dihydroquinolin-4(1H)-one

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Chemical Property of 3-(Bis(methylthio)methyl)-1-(4-chlorophenylsulfonyl)-2,3-dihydroquinolin-4(1H)-one

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Technology Process of 3-(Bis(methylthio)methyl)-1-(4-chlorophenylsulfonyl)-2,3-dihydroquinolin-4(1H)-one

There total 1 articles about 3-(Bis(methylthio)methyl)-1-(4-chlorophenylsulfonyl)-2,3-dihydroquinolin-4(1H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 959995-86-9
1-(4-Chlorophenylsulfonyl)-2,3-dihydroquinolin-4(1H)-one

: 74-88-4
methyl iodide

: 959996-88-4
3-(Bis(methylthio)methyl)-1-(4-chlorophenylsulfonyl)-2,3-dihydroquinolin-4(1H)-one

Guidance literature:: carbon disulfide; 1-(4-Chlorophenylsulfonyl)-2,3-dihydroquinolin-4(1H)-one; With potassium tert-butylate; In tetrahydrofuran; for 0.75h;

methyl iodide; In tetrahydrofuran; at 20 ℃; for 1.5h;

Reference yield: 66.0%

: 959996-88-4
3-(Bis(methylthio)methyl)-1-(4-chlorophenylsulfonyl)-2,3-dihydroquinolin-4(1H)-one

: 5-[(4-chlorophenyl)sulfonyl]-3-(methylthio)-4,5-dihydro-1H-pyrazolo[4,3-c]quinoline

Guidance literature:: With hydrazine; In tetrahydrofuran; ethanol; for 4h;

Reference yield:

: 959996-88-4
3-(Bis(methylthio)methyl)-1-(4-chlorophenylsulfonyl)-2,3-dihydroquinolin-4(1H)-one

: 50-01-1
guanidine hydrochloride

: 959996-90-8
6-(4-chlorophenylsulfonyl)-4-methoxy-5,6-dihydropyrimido[5,4-c]quinolin-2-amine

Guidance literature:: 3-(Bis(methylthio)methyl)-1-(4-chlorophenylsulfonyl)-2,3-dihydroquinolin-4(1H)-one; guanidine hydrochloride; In methanol; for 16h;

With sodium hydrogencarbonate; In methanol; for 21h; Heating / reflux;