Technology Process of <(2S,3S)-2-(benzyloxy)-8-hydroxynon-3-yl>-p-toluenesulfonate
There total 5 articles about <(2S,3S)-2-(benzyloxy)-8-hydroxynon-3-yl>-p-toluenesulfonate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium aluminium tetrahydride;
In
tetrahydrofuran; diethyl ether;
for 1h;
Ambient temperature;
DOI:10.1021/jm00048a020
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 96 percent / Li2CuCl4 / diethyl ether / 1 h / -78 °C
2: 97 percent / pyridine / 12 h / Ambient temperature
3: 99 percent / 85percent m-chloroperbenzoic acid / CH2Cl2 / Ambient temperature
4: 95 percent / 1 M LAH / tetrahydrofuran; diethyl ether / 1 h / Ambient temperature
With
pyridine; lithium aluminium tetrahydride; dilithium tetrachlorocuprate; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/jm00048a020
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 96 percent / Li2CuCl4 / diethyl ether / 1 h / -78 °C
2: 97 percent / pyridine / 12 h / Ambient temperature
3: 99 percent / 85percent m-chloroperbenzoic acid / CH2Cl2 / Ambient temperature
4: 95 percent / 1 M LAH / tetrahydrofuran; diethyl ether / 1 h / Ambient temperature
With
pyridine; lithium aluminium tetrahydride; dilithium tetrachlorocuprate; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/jm00048a020
