2-[3,4-Bis-(tert-butyl-dimethyl-silanyloxy)-phenyl]-2-(2-nitro-phenylselanyl)-ethylamine

Base Information

Chemical Name:2-[3,4-Bis-(tert-butyl-dimethyl-silanyloxy)-phenyl]-2-(2-nitro-phenylselanyl)-ethylamine
CAS No.:132268-35-0
Molecular Formula:C₂₆H₄₂N₂O₄SeSi₂
Molecular Weight:581.761
Hs Code.:

Synonyms:2-[3,4-Bis-(tert-butyl-dimethyl-silanyloxy)-phenyl]-2-(2-nitro-phenylselanyl)-ethylamine

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Chemical Property of 2-[3,4-Bis-(tert-butyl-dimethyl-silanyloxy)-phenyl]-2-(2-nitro-phenylselanyl)-ethylamine

Chemical Property:

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Technology Process of 2-[3,4-Bis-(tert-butyl-dimethyl-silanyloxy)-phenyl]-2-(2-nitro-phenylselanyl)-ethylamine

There total 8 articles about 2-[3,4-Bis-(tert-butyl-dimethyl-silanyloxy)-phenyl]-2-(2-nitro-phenylselanyl)-ethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 132245-83-1
[2-[3,4-Bis-(tert-butyl-dimethyl-silanyloxy)-phenyl]-2-(2-nitro-phenylselanyl)-ethyl]-carbamic acid tert-butyl ester

: 132268-35-0
2-[3,4-Bis-(tert-butyl-dimethyl-silanyloxy)-phenyl]-2-(2-nitro-phenylselanyl)-ethylamine

Guidance literature:: With trifluoroacetic acid; In dichloromethane;
DOI:10.1016/S0040-4039(00)97256-3

Reference yield:

: 51694-22-5
ortho-nitrophenyl selenocyanate

: 132268-35-0
2-[3,4-Bis-(tert-butyl-dimethyl-silanyloxy)-phenyl]-2-(2-nitro-phenylselanyl)-ethylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / n-Bu₃P / tetrahydrofuran

2: 100 percent / 30percent TFA / CH₂Cl₂

With tributylphosphine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4039(00)97256-3

Reference yield:

: 99815-16-4
3,4-bis(tert-butyldimethylsilanyloxy)benzaldehyde

: 132268-35-0
2-[3,4-Bis-(tert-butyl-dimethyl-silanyloxy)-phenyl]-2-(2-nitro-phenylselanyl)-ethylamine

Guidance literature:: Multi-step reaction with 5 steps

1: 100 percent / ZnI₂

2: LiAlH₄ / tetrahydrofuran

3: CH₂Cl₂

4: 75 percent / n-Bu₃P / tetrahydrofuran

5: 100 percent / 30percent TFA / CH₂Cl₂

With lithium aluminium tetrahydride; tributylphosphine; trifluoroacetic acid; zinc(II) iodide; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4039(00)97256-3