<1-(Methylthio)-2,2-diphenylvinyl>vinylsulfon

Base Information

Chemical Name:<1-(Methylthio)-2,2-diphenylvinyl>vinylsulfon
CAS No.:113354-29-3
Molecular Formula:C₁₇H₁₆O₂S₂
Molecular Weight:316.445
Hs Code.:

Synonyms:<1-(Methylthio)-2,2-diphenylvinyl>vinylsulfon

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Chemical Property of <1-(Methylthio)-2,2-diphenylvinyl>vinylsulfon

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Technology Process of <1-(Methylthio)-2,2-diphenylvinyl>vinylsulfon

There total 4 articles about <1-(Methylthio)-2,2-diphenylvinyl>vinylsulfon which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 113354-09-9
2-(Diphenylmethylen)-1,3-dithiolan-S,S-dioxid

: 74-88-4
methyl iodide

: 113354-29-3
<1-(Methylthio)-2,2-diphenylvinyl>vinylsulfon

Guidance literature:: With potassium tert-butylate; at -78 ℃;

Reference yield:

: 67951-97-7
2-(Diphenylmethylen)-1,3-dithiolan

: 113354-29-3
<1-(Methylthio)-2,2-diphenylvinyl>vinylsulfon

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / 60percent 3-chloroperbenzoic acid

2: 89 percent / KMnO₄ / CH₃(C₈H₁₇)3N(+)Cl(-), MgSO₄ / CH₂Cl₂; H₂O / 0.5 h / Ambient temperature

3: 1) base / 1) -78 deg C, 10 min

With potassium permanganate; 3-chloro-benzenecarboperoxoic acid; magnesium sulfate; In dichloromethane; water;

Reference yield:

: 117-34-0
2,2-diphenylacetic acid

: 113354-29-3
<1-(Methylthio)-2,2-diphenylvinyl>vinylsulfon

Guidance literature:: Multi-step reaction with 4 steps

1: 35 percent / TiCl₄ / CCl₄ / 0.5 h / Heating

2: 81 percent / 60percent 3-chloroperbenzoic acid

3: 89 percent / KMnO₄ / CH₃(C₈H₁₇)3N(+)Cl(-), MgSO₄ / CH₂Cl₂; H₂O / 0.5 h / Ambient temperature

4: 1) base / 1) -78 deg C, 10 min

With potassium permanganate; titanium tetrachloride; 3-chloro-benzenecarboperoxoic acid; magnesium sulfate; In tetrachloromethane; dichloromethane; water;