Technology Process of C9H6Cl3F3O
There total 3 articles about C9H6Cl3F3O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
caesium carbonate; N,N-dimethyl-formamide; sodium iodide;
at 22 ℃;
for 16h;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: phosphorus tribromide / dichloromethane / 2 h / 0 - 22 °C
2: caesium carbonate; sodium iodide; N,N-dimethyl-formamide / 16 h / 22 °C
With
phosphorus tribromide; caesium carbonate; N,N-dimethyl-formamide; sodium iodide;
In
dichloromethane;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: borane-dimethyl sulfide complex / tetrahydrofuran / 22 °C / Inert atmosphere; Cooling with ice; Reflux
2: phosphorus tribromide / dichloromethane / 2 h / 0 - 22 °C
3: caesium carbonate; sodium iodide; N,N-dimethyl-formamide / 16 h / 22 °C
With
borane-dimethyl sulfide complex; phosphorus tribromide; caesium carbonate; N,N-dimethyl-formamide; sodium iodide;
In
tetrahydrofuran; dichloromethane;